methyl 2-deoxy-3,4-O-isopropylidene-5-iodo-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate

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Chemical Name:methyl 2-deoxy-3,4-O-isopropylidene-5-iodo-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate
CAS No.:404369-19-3
Molecular Formula:C₂₈H₂₈INO₄
Molecular Weight:569.439
Hs Code.:

Synonyms:methyl 2-deoxy-3,4-O-isopropylidene-5-iodo-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate

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Chemical Property of methyl 2-deoxy-3,4-O-isopropylidene-5-iodo-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate

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Technology Process of methyl 2-deoxy-3,4-O-isopropylidene-5-iodo-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate

There total 4 articles about methyl 2-deoxy-3,4-O-isopropylidene-5-iodo-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 214619-42-8
methyl 2-deoxy-3,4-O-isopropylidene-5-O-methanesulfonyl-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate

: 404369-19-3
methyl 2-deoxy-3,4-O-isopropylidene-5-iodo-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate

Guidance literature:: With lithium iodide; In N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1016/S0040-4020(01)01070-5

Reference yield:

: 154494-79-8
methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-mannonate

: 404369-19-3
methyl 2-deoxy-3,4-O-isopropylidene-5-iodo-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate

Guidance literature:: Multi-step reaction with 4 steps

1: NaIO₄ / ethanol; H₂O / 3 h / 20 °C

2: 5.52 g / NaNH₄ / ethanol; H₂O / 0.17 h / 0 °C

3: 98 percent / Et₃N / tetrahydrofuran / 0.33 h / 20 °C

4: 95 percent / LiI / dimethylformamide / 80 °C

With sodium periodate; triethylamine; lithium iodide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)01070-5

Reference yield:

: 214619-41-7
methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate

: 404369-19-3
methyl 2-deoxy-3,4-O-isopropylidene-5-iodo-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / tetrahydrofuran / 0.33 h / 20 °C

2: 95 percent / LiI / dimethylformamide / 80 °C

With triethylamine; lithium iodide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)01070-5