1-methyl-2-diphenylphosphino-3-methylimidazolium hexafluorophosphate

Base Information

Chemical Name:1-methyl-2-diphenylphosphino-3-methylimidazolium hexafluorophosphate
CAS No.:1104626-24-5
Molecular Formula:C₁₇H₁₈N₂P*F₆P
Molecular Weight:426.281
Hs Code.:

Synonyms:1-methyl-2-diphenylphosphino-3-methylimidazolium hexafluorophosphate

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Chemical Property of 1-methyl-2-diphenylphosphino-3-methylimidazolium hexafluorophosphate

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Technology Process of 1-methyl-2-diphenylphosphino-3-methylimidazolium hexafluorophosphate

There total 1 articles about 1-methyl-2-diphenylphosphino-3-methylimidazolium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121091-36-9
2-diphenylphosphine-N,N-dimethylimidazolium chloride

: 1104626-24-5
1-methyl-2-diphenylphosphino-3-methylimidazolium hexafluorophosphate

Guidance literature:: With potassium hexafluorophosphate; Inert atmosphere;
DOI:10.1002/adsc.200900133

Reference yield: 99.0%

: chloro(1,5-cyclooctadiene)rhodium(I) dimer

: 1104626-24-5
1-methyl-2-diphenylphosphino-3-methylimidazolium hexafluorophosphate

: (C₃H₂(NCH₃)2PPPh₂)chlororhodium(I)(1,5-cyclooctadiene) hexafluorophosphate

Guidance literature:: In dichloromethane; (Ar), ligand and Rh complex (2:1) in CH2Cl2 stirred at room temp. for 3 h; evapd.(vac.), elem. anal.;
DOI:10.1016/j.inoche.2008.09.004

Reference yield: 99.0%

: chloro(1,5-cyclooctadiene)rhodium(I) dimer

: 1104626-24-5
1-methyl-2-diphenylphosphino-3-methylimidazolium hexafluorophosphate

: 201230-82-2
carbon monoxide

: (C₃H₂(NCH₃)2PPPh₂)2 chlorocarbonylrhodium(I) hexafluorophosphate

Guidance literature:: In dichloromethane; toluene; (Ar), soln. of Rh complex in toluene treated with 4 equiv. of ligand in CH2Cl2, CO introdused in soln. for 15 min, stirred overnight at room temp.; filtered, ppt. washed (pentane), dried (vac.), elem. anal.;
DOI:10.1016/j.inoche.2008.09.004