mono(1-(4-prop-2-ynyloxy-phenyl)-2-methoxycarbonyl-2-propenyl)glutaric acid N-hydroxy succinimide ester

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Chemical Name:mono(1-(4-prop-2-ynyloxy-phenyl)-2-methoxycarbonyl-2-propenyl)glutaric acid N-hydroxy succinimide ester
CAS No.:1456890-65-5
Molecular Formula:C₂₃H₂₃NO₉
Molecular Weight:457.437
Hs Code.:

Synonyms:mono(1-(4-prop-2-ynyloxy-phenyl)-2-methoxycarbonyl-2-propenyl)glutaric acid N-hydroxy succinimide ester

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Chemical Property of mono(1-(4-prop-2-ynyloxy-phenyl)-2-methoxycarbonyl-2-propenyl)glutaric acid N-hydroxy succinimide ester

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Technology Process of mono(1-(4-prop-2-ynyloxy-phenyl)-2-methoxycarbonyl-2-propenyl)glutaric acid N-hydroxy succinimide ester

There total 5 articles about mono(1-(4-prop-2-ynyloxy-phenyl)-2-methoxycarbonyl-2-propenyl)glutaric acid N-hydroxy succinimide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1456890-64-4
methyl 2-[hydroxy-(4-prop-2-ynyloxy-phenyl)-methyl]acrylate

: 117746-42-6
5-[(2',5'-dioxo-1'-pyrrolidinyl)oxy]-5-oxopentanoyl chloride

: 1456890-65-5
mono(1-(4-prop-2-ynyloxy-phenyl)-2-methoxycarbonyl-2-propenyl)glutaric acid N-hydroxy succinimide ester

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 4h;

Reference yield:

: 5-[(2,5-dioxopyrrolidin-1-yl)oxy]-5-oxopentanoic acid

: 1456890-65-5
mono(1-(4-prop-2-ynyloxy-phenyl)-2-methoxycarbonyl-2-propenyl)glutaric acid N-hydroxy succinimide ester

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C

2: pyridine / dichloromethane / 4 h / 0 - 20 °C

With pyridine; thionyl chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3cc43271h

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1456890-65-5
mono(1-(4-prop-2-ynyloxy-phenyl)-2-methoxycarbonyl-2-propenyl)glutaric acid N-hydroxy succinimide ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 6 h / Reflux

2: 1,4-diaza-bicyclo[2.2.2]octane / methanol / 48 h / 20 °C / Darkness

3: pyridine / dichloromethane / 4 h / 0 - 20 °C

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; potassium carbonate; In methanol; dichloromethane; acetone;
DOI:10.1039/c3cc43271h