1-isopropyl-4-methoxyphenylethyl iodide

Base Information

Chemical Name:1-isopropyl-4-methoxyphenylethyl iodide
CAS No.:187161-50-8
Molecular Formula:C₁₂H₁₇IO
Molecular Weight:304.171
Hs Code.:

Synonyms:1-isopropyl-4-methoxyphenylethyl iodide

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Chemical Property of 1-isopropyl-4-methoxyphenylethyl iodide

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Technology Process of 1-isopropyl-4-methoxyphenylethyl iodide

There total 6 articles about 1-isopropyl-4-methoxyphenylethyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 39863-70-2
2-(3-isopropyl-4-methoxyphenyl)ethan-1-ol

: 187161-50-8
1-isopropyl-4-methoxyphenylethyl iodide

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In diethyl ether; acetonitrile; at 0 ℃;
DOI:10.1080/00397919708005040

Reference yield:

: 702-23-8
2-(4-Methoxyphenyl)ethanol

: 187161-50-8
1-isopropyl-4-methoxyphenylethyl iodide

Guidance literature:: Multi-step reaction with 6 steps

1: 4.54 g / AlCl₃ / CH₂Cl₂ / Ambient temperature

2: 4.54 g / diethyl ether / 1 h / Heating

3: 4.53 g / 2 h / Heating

4: 3.08 g / H₂ / Pd/C / diethyl ether / 20 h / 1551.4 Torr

5: 2.50 g / aq. NaOH / methanol

6: 90 percent / I₂, PPh₃, imidazole / acetonitrile; diethyl ether / 0 °C

With 1H-imidazole; sodium hydroxide; aluminium trichloride; hydrogen; iodine; triphenylphosphine; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1080/00397919708005040

Reference yield:

: 134435-46-4
3-acetyl-4-methoxyphenylethyl acetate

: 187161-50-8
1-isopropyl-4-methoxyphenylethyl iodide

Guidance literature:: Multi-step reaction with 5 steps

1: 4.54 g / diethyl ether / 1 h / Heating

2: 4.53 g / 2 h / Heating

3: 3.08 g / H₂ / Pd/C / diethyl ether / 20 h / 1551.4 Torr

4: 2.50 g / aq. NaOH / methanol

5: 90 percent / I₂, PPh₃, imidazole / acetonitrile; diethyl ether / 0 °C

With 1H-imidazole; sodium hydroxide; hydrogen; iodine; triphenylphosphine; palladium on activated charcoal; In methanol; diethyl ether; acetonitrile;
DOI:10.1080/00397919708005040