Technology Process of C10H12BrNO
There total 4 articles about C10H12BrNO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C15H20BrNO3;
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
With
sodium hydroxide;
In
ethyl acetate;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide; ethanol / 60 °C
2.1: triethylamine; diphenylphosphoranyl azide / 20 °C / Reflux
3.1: trifluoroacetic acid / dichloromethane / 20 °C
3.2: 0.5 h
With
ethanol; diphenylphosphoranyl azide; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 60 °C
2.1: sodium hydroxide; ethanol / 60 °C
3.1: triethylamine; diphenylphosphoranyl azide / 20 °C / Reflux
4.1: trifluoroacetic acid / dichloromethane / 20 °C
4.2: 0.5 h
With
ethanol; diphenylphosphoranyl azide; potassium carbonate; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
dichloromethane; N,N-dimethyl-formamide;