Technology Process of C36H51NO5
There total 6 articles about C36H51NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 24.3333h;
Inert atmosphere;
DOI:10.1016/j.steroids.2011.10.009
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuric acid / water; acetic acid / 2 h / Reflux; Inert atmosphere
2: methanol; water; potassium hydroxide / 2 h / 20 °C / Inert atmosphere
3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 24.33 h / 0 - 20 °C / Inert atmosphere
With
methanol; sulfuric acid; water; triphenylphosphine; potassium hydroxide; diethylazodicarboxylate;
In
tetrahydrofuran; water; acetic acid;
3: Mitsunobu reaction;
DOI:10.1016/j.steroids.2011.10.009
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium hydrogencarbonate / acetone / 6 h / Inert atmosphere; Reflux
2: Jones reagent / acetone / 0.08 h / 0 °C / Inert atmosphere
3: sulfuric acid / water; acetic acid / 2 h / Reflux; Inert atmosphere
4: methanol; water; potassium hydroxide / 2 h / 20 °C / Inert atmosphere
5: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 24.33 h / 0 - 20 °C / Inert atmosphere
With
methanol; Jones reagent; sulfuric acid; water; potassium hydrogencarbonate; triphenylphosphine; potassium hydroxide; diethylazodicarboxylate;
In
tetrahydrofuran; water; acetic acid; acetone;
5: Mitsunobu reaction;
DOI:10.1016/j.steroids.2011.10.009
