(3-{3-[hydroxy-bis-(4-methoxy-phenyl)-methyl]-phenoxy}-phenyl)-bis-(4-methoxy-phenyl)-methanol

Base Information

Chemical Name:(3-{3-[hydroxy-bis-(4-methoxy-phenyl)-methyl]-phenoxy}-phenyl)-bis-(4-methoxy-phenyl)-methanol
CAS No.:724422-73-5
Molecular Formula:C₄₂H₃₈O₇
Molecular Weight:654.76
Hs Code.:

Synonyms:(3-{3-[hydroxy-bis-(4-methoxy-phenyl)-methyl]-phenoxy}-phenyl)-bis-(4-methoxy-phenyl)-methanol

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Chemical Property of (3-{3-[hydroxy-bis-(4-methoxy-phenyl)-methyl]-phenoxy}-phenyl)-bis-(4-methoxy-phenyl)-methanol

Chemical Property:

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Technology Process of (3-{3-[hydroxy-bis-(4-methoxy-phenyl)-methyl]-phenoxy}-phenyl)-bis-(4-methoxy-phenyl)-methanol

There total 3 articles about (3-{3-[hydroxy-bis-(4-methoxy-phenyl)-methyl]-phenoxy}-phenyl)-bis-(4-methoxy-phenyl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 724422-72-4
C₁₈H₁₈O₅

: 724422-73-5
(3-{3-[hydroxy-bis-(4-methoxy-phenyl)-methyl]-phenoxy}-phenyl)-bis-(4-methoxy-phenyl)-methanol

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 18h;
DOI:10.1016/j.bmcl.2004.03.097

Reference yield:

: 535-80-8
3-chlorobenzoate

: 724422-73-5
(3-{3-[hydroxy-bis-(4-methoxy-phenyl)-methyl]-phenoxy}-phenyl)-bis-(4-methoxy-phenyl)-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 49 percent / K₂CO₃; CuCl; 8-quinolinol / tris[2-(2-methoxyethoxy)ethyl]amine / various solvent(s) / 12 h / 170 °C

2: 73 percent / H₂SO₄ / 36 h / Heating

3: 99 percent / tetrahydrofuran / 18 h / 20 °C

With 8-quinolinol; sulfuric acid; potassium carbonate; copper(l) chloride; Tris(3,6-dioxaheptyl)amine; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2004.03.097

Reference yield:

: 15791-89-6
3,3'-oxy-di-benzoic acid

: 724422-73-5
(3-{3-[hydroxy-bis-(4-methoxy-phenyl)-methyl]-phenoxy}-phenyl)-bis-(4-methoxy-phenyl)-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / H₂SO₄ / 36 h / Heating

2: 99 percent / tetrahydrofuran / 18 h / 20 °C

With sulfuric acid; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2004.03.097