lithium <(phenylsulfonyl)methylene>nitronate

Base Information

Chemical Name:lithium <(phenylsulfonyl)methylene>nitronate
CAS No.:74738-03-7
Molecular Formula:C₇H₆NO₄S*Li
Molecular Weight:207.136
Hs Code.:

Synonyms:lithium <(phenylsulfonyl)methylene>nitronate

Suppliers and Price of lithium <(phenylsulfonyl)methylene>nitronate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of lithium <(phenylsulfonyl)methylene>nitronate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of lithium <(phenylsulfonyl)methylene>nitronate

There total 4 articles about lithium <(phenylsulfonyl)methylene>nitronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 21272-85-5
phenylsulfonylnitromethane

: 74738-03-7
lithium <(phenylsulfonyl)methylene>nitronate

Guidance literature:: With lithium methanolate; In methanol; dichloromethane;
DOI:10.1021/jo00317a023

Reference yield:

: 873-55-2
sodium benzenesulfonate

: 74738-03-7
lithium <(phenylsulfonyl)methylene>nitronate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaOMe; 2) I₂ / 1) DMF, 10 min, cooling bath; 2) 1h

2: 93 percent / LiOMe / CH₂Cl₂; methanol

With lithium methanolate; iodine; sodium methylate; In methanol; dichloromethane;
DOI:10.1021/jo00317a023

Reference yield:

: 100-39-0
benzyl bromide

: 74738-03-7
lithium <(phenylsulfonyl)methylene>nitronate

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / dimethylsulfoxide / 24 h

2: 93 percent / LiOMe / CH₂Cl₂; methanol

With lithium methanolate; In methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jo00317a023