N-(benzyloxycarbonyl)-L-valine N-hydroxy-5-norbornene-2,3-dicarboximide ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)-L-valine N-hydroxy-5-norbornene-2,3-dicarboximide ester
CAS No.:53666-01-6
Molecular Formula:C₂₂H₂₄N₂O₆
Molecular Weight:412.442
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-L-valine N-hydroxy-5-norbornene-2,3-dicarboximide ester

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Chemical Property of N-(benzyloxycarbonyl)-L-valine N-hydroxy-5-norbornene-2,3-dicarboximide ester

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Technology Process of N-(benzyloxycarbonyl)-L-valine N-hydroxy-5-norbornene-2,3-dicarboximide ester

There total 7 articles about N-(benzyloxycarbonyl)-L-valine N-hydroxy-5-norbornene-2,3-dicarboximide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 137283-63-7
Carbonic acid 3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl ester isopropenyl ester

: 53666-01-6
N-(benzyloxycarbonyl)-L-valine N-hydroxy-5-norbornene-2,3-dicarboximide ester

Guidance literature:: With dmap; In acetonitrile; for 4h; Ambient temperature;
DOI:10.1055/s-1991-26545

Reference yield:

: 21715-90-2
N-hydroxy-5-norbornene-2,3-dicarboximide

: 53666-01-6
N-(benzyloxycarbonyl)-L-valine N-hydroxy-5-norbornene-2,3-dicarboximide ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / acetonitrile; acetone / 0 °C

2: 99 percent / DMAP / acetonitrile / 4 h / Ambient temperature

With dmap; triethylamine; In acetone; acetonitrile;
DOI:10.1055/s-1991-26545