C₄₂H₅₀O₁₄

Base Information

• Chemical Name: C₄₂H₅₀O₁₄
• CAS No.: 1384545-96-3
• Molecular Formula: C₄₂H₅₀O₁₄
• Molecular Weight: 778.851
• Mol file: 1384545-96-3.mol

Synonyms:C₄₂H₅₀O₁₄

Chemical Property of C₄₂H₅₀O₁₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₂H₅₀O₁₄

There total 10 articles about C₄₂H₅₀O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

C27H36O11 (1384545-88-3) + 3,4-di-O-allyl caffeic acid chloride (797041-01-1) → C42H50O14 (1384545-96-3)

Guidance literature:

With dmap; triethylamine; In dichloromethane; for 36h; Reflux;

DOI:10.1039/c2ob25124h

Reference yield:

(E)-3-methoxy-4-allyloxycinnamoyl chloride (850786-96-8) → C42H50O14 (1384545-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; dmap / dichloromethane / 24 h / Reflux

2: dmap; triethylamine / dichloromethane / 36 h / Reflux

With pyridine; dmap; triethylamine; In dichloromethane;

DOI:10.1039/c2ob25124h

Reference yield:

caffeic acid (331-39-5,501-16-6) → C42H50O14 (1384545-96-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 0.5 h / 20 °C

1.2: 48 h / Reflux

1.3: 2 h / Reflux

2.1: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 10 h / 0 - 20 °C

3.1: dmap; triethylamine / dichloromethane / 36 h / Reflux

With dmap; oxalyl dichloride; potassium carbonate; triethylamine; N,N-dimethyl-formamide; In dichloromethane; acetone; toluene; 1.2: Williamson ether synthesis;

DOI:10.1039/c2ob25124h

upstream raw materials:

C₂₇H₃₆O₁₁

3,4-di-O-allyl caffeic acid chloride

(E)-3-methoxy-4-allyloxycinnamoyl chloride

(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid

Downstream raw materials:

methyl 1-O-caffeoyl-3-O-feruloyl-muco-quinate