Technology Process of C27H47ClO3S
There total 5 articles about C27H47ClO3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Octanethiol;
With
sodium t-butanolate;
In
methanol;
at 20 ℃;
for 0.5h;
1-[2,5-bis(chloromethyl)-4-methoxyphenoxy]-3,7-dimethyloctane bis(tetrathiophenium);
In
methanol;
at 20 ℃;
for 3h;
Inert atmosphere;
With
hydrogenchloride; tellurium oxide; dihydrogen peroxide;
In
1,4-dioxane; water;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; acetic anhydride / water / 4 h / 20 - 70 °C / Inert atmosphere
2.1: potassium hydroxide / methanol / 72 h / 20 °C / Inert atmosphere
3.1: sodium t-butanolate / methanol / 0.5 h / 20 °C
3.2: 3 h / 20 °C / Inert atmosphere
3.3: Inert atmosphere
With
hydrogenchloride; acetic anhydride; potassium hydroxide; sodium t-butanolate;
In
methanol; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium hydroxide / dichloromethane; chloroform; nitrogen / 3 h / 0 - 5 °C / Inert atmosphere; liquid N2
2.1: sodium t-butanolate / ethanol / 1 h / 20 °C / Inert atmosphere
2.2: 80 °C
3.1: hydrogenchloride; acetic anhydride / water / 4 h / 20 - 70 °C / Inert atmosphere
4.1: potassium hydroxide / methanol / 72 h / 20 °C / Inert atmosphere
5.1: sodium t-butanolate / methanol / 0.5 h / 20 °C
5.2: 3 h / 20 °C / Inert atmosphere
5.3: Inert atmosphere
With
hydrogenchloride; acetic anhydride; potassium hydroxide; sodium t-butanolate;
In
methanol; ethanol; dichloromethane; chloroform; nitrogen; water;
