(1S,2S,4R,1'R,2'S,4'S)-2-Hydroxy-[2,2']bi[bicyclo[2.2.1]heptyl]-5,5'-diene-3,3'-dione 3-oxime

Base Information

Chemical Name:(1S,2S,4R,1'R,2'S,4'S)-2-Hydroxy-[2,2']bi[bicyclo[2.2.1]heptyl]-5,5'-diene-3,3'-dione 3-oxime
CAS No.:131515-75-8
Molecular Formula:C₁₄H₁₅NO₃
Molecular Weight:245.278
Hs Code.:

Synonyms:(1S,2S,4R,1'R,2'S,4'S)-2-Hydroxy-[2,2']bi[bicyclo[2.2.1]heptyl]-5,5'-diene-3,3'-dione 3-oxime

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Chemical Property of (1S,2S,4R,1'R,2'S,4'S)-2-Hydroxy-[2,2']bi[bicyclo[2.2.1]heptyl]-5,5'-diene-3,3'-dione 3-oxime

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Technology Process of (1S,2S,4R,1'R,2'S,4'S)-2-Hydroxy-[2,2']bi[bicyclo[2.2.1]heptyl]-5,5'-diene-3,3'-dione 3-oxime

There total 2 articles about (1S,2S,4R,1'R,2'S,4'S)-2-Hydroxy-[2,2']bi[bicyclo[2.2.1]heptyl]-5,5'-diene-3,3'-dione 3-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 694-98-4
norborn-5-en-2-one

: 176714-60-6
Bicyclo<2.2.1>hept-5-ene-2,3-dione monoxime

: 131515-75-8
(1S,2S,4R,1'R,2'S,4'S)-2-Hydroxy-[2,2']bi[bicyclo[2.2.1]heptyl]-5,5'-diene-3,3'-dione 3-oxime

: 131515-72-5,131613-32-6
(1S,4R)-4-(Hydroxyimino-methyl)-cyclopent-2-enecarboxylic acid ethyl ester

: 104323-62-8,133161-66-7,133161-76-9,133161-77-0,133161-78-1,133161-79-2,133267-34-2
2'-Hydroxy-[2,2']bi[bicyclo[2.2.1]heptyl]-5,5'-dien-3-one

Guidance literature:: With n-butyllithium; ethyl nitrite; diisopropylamine; Multistep reaction; 1) THF, -78 deg C then r.t. 2) THF, -78 deg C;
DOI:10.1021/jo00002a040

Reference yield: 12.0%

: 109-95-5
ethyl nitrite

: 694-98-4
norborn-5-en-2-one

: 176714-60-6
Bicyclo<2.2.1>hept-5-ene-2,3-dione monoxime

: 131515-75-8
(1S,2S,4R,1'R,2'S,4'S)-2-Hydroxy-[2,2']bi[bicyclo[2.2.1]heptyl]-5,5'-diene-3,3'-dione 3-oxime

: 131515-72-5,131613-32-6
(1S,4R)-4-(Hydroxyimino-methyl)-cyclopent-2-enecarboxylic acid ethyl ester

: 104323-62-8,133161-66-7,133161-76-9,133161-77-0,133161-78-1,133161-79-2,133267-34-2
2'-Hydroxy-[2,2']bi[bicyclo[2.2.1]heptyl]-5,5'-dien-3-one

Guidance literature:: With n-butyllithium; diisopropylamine; Multistep reaction; 1) THF, -78 deg C then r.t. 2) THF, -78 deg C;
DOI:10.1021/jo00002a040