(S)-1-Methyl-4-(p-tolylsulfonyl)butyl 4-chlorobutanoate

Base Information

Chemical Name:(S)-1-Methyl-4-(p-tolylsulfonyl)butyl 4-chlorobutanoate
CAS No.:155729-12-7
Molecular Formula:C₁₆H₂₃ClO₄S
Molecular Weight:346.875
Hs Code.:

Synonyms:(S)-1-Methyl-4-(p-tolylsulfonyl)butyl 4-chlorobutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-Methyl-4-(p-tolylsulfonyl)butyl 4-chlorobutanoate

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Technology Process of (S)-1-Methyl-4-(p-tolylsulfonyl)butyl 4-chlorobutanoate

There total 2 articles about (S)-1-Methyl-4-(p-tolylsulfonyl)butyl 4-chlorobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 131701-87-6
(S)-(-)-5-p-toluenesulfonylpentane-2-ol

: 4635-59-0
4-Chlorobutanoyl chloride

: 155729-12-7
(S)-1-Methyl-4-(p-tolylsulfonyl)butyl 4-chlorobutanoate

Guidance literature:: With triethylamine; In diethyl ether; Ambient temperature;
DOI:10.1021/jo00087a014

Reference yield:

: 82275-99-8
5-(Toluene-4-sulfonyl)-pentan-2-one

: 155729-12-7
(S)-1-Methyl-4-(p-tolylsulfonyl)butyl 4-chlorobutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: baker's yeast reduction

2: 88 percent / Et₃N / diethyl ether / Ambient temperature

With triethylamine; In diethyl ether;
DOI:10.1021/jo00087a014

Reference yield:

: 155729-12-7
(S)-1-Methyl-4-(p-tolylsulfonyl)butyl 4-chlorobutanoate

: (S)-2-(Chloropropyl)-6-methyl-3-(p-tolylsulfonyl)-5,6-dihydropyran

Guidance literature:: With toluene-4-sulfonic acid; lithium hexamethyldisilazane; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 2.) benzene, 3 h;
DOI:10.1021/jo00087a014