(R)-3-((R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-octanoic acid methyl ester

Base Information

Chemical Name:(R)-3-((R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-octanoic acid methyl ester
CAS No.:115482-38-7
Molecular Formula:C₁₉H₂₅F₃O₅
Molecular Weight:390.4
Hs Code.:

Synonyms:(R)-3-((R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-octanoic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-3-((R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-octanoic acid methyl ester

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Technology Process of (R)-3-((R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-octanoic acid methyl ester

There total 2 articles about (R)-3-((R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-octanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 20445-31-2
R-(+)-α-trifluoromethyl-α-methoxy-phenylacetic acid

: 78672-90-9,85549-54-8
methyl (R)-(-)-3-hydroxydecanoate

: 115482-38-7
(R)-3-((R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-octanoic acid methyl ester

Guidance literature:: With dmap; diisopropyl-carbodiimide; In dichloromethane; for 8h;
DOI:10.1021/ja00226a041

Reference yield:

: 62344-14-3
(E)-methyl 3-oxo-6-octenoate

: 115482-38-7
(R)-3-((R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-octanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / hydrogen / Ru₂Cl₄<(R)-binap>2Et₃N / methanol / 48 h / 76000 Torr / Ambient temperature

2: 95 percent / DMAP, 1,3-diisopropylcarbodiimide / CH₂Cl₂ / 8 h

With dmap; hydrogen; diisopropyl-carbodiimide; <((R)-(1,1'-binaphthyl-2,2'-diyl)bis(diphenylphosphine))RuCl2>2NEt3; In methanol; dichloromethane;
DOI:10.1021/ja00226a041