3,5-dichlorobenzyl 4-{2-[(1H-benzotriazole-5-carbonyl)amino]-ethyl}piperazine-1-carboxylate

Base Information

Chemical Name:3,5-dichlorobenzyl 4-{2-[(1H-benzotriazole-5-carbonyl)amino]-ethyl}piperazine-1-carboxylate
CAS No.:1246639-64-4
Molecular Formula:C₂₁H₂₂Cl₂N₆O₃
Molecular Weight:477.35
Hs Code.:

Synonyms:3,5-dichlorobenzyl 4-{2-[(1H-benzotriazole-5-carbonyl)amino]-ethyl}piperazine-1-carboxylate

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Chemical Property of 3,5-dichlorobenzyl 4-{2-[(1H-benzotriazole-5-carbonyl)amino]-ethyl}piperazine-1-carboxylate

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Technology Process of 3,5-dichlorobenzyl 4-{2-[(1H-benzotriazole-5-carbonyl)amino]-ethyl}piperazine-1-carboxylate

There total 4 articles about 3,5-dichlorobenzyl 4-{2-[(1H-benzotriazole-5-carbonyl)amino]-ethyl}piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 60211-57-6
3,5-dichlorobenzyl alcohol

: 1246639-93-9
C₁₃H₁₈N₆O*ClH

: 530-62-1
1,1'-carbonyldiimidazole

: 1246639-64-4
3,5-dichlorobenzyl 4-{2-[(1H-benzotriazole-5-carbonyl)amino]-ethyl}piperazine-1-carboxylate

Guidance literature:: 3,5-dichlorobenzyl alcohol; 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

C₁₃H₁₈N₆O*ClH; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

: 192130-34-0
tert-butyl 4-(2-aminoethyl)piperazine-1-carboxylate

: 1246639-64-4
3,5-dichlorobenzyl 4-{2-[(1H-benzotriazole-5-carbonyl)amino]-ethyl}piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 4-methyl-morpholine / N,N-dimethyl-formamide / 18 h / 20 °C

2.1: hydrogenchloride; isopropyl alcohol / 2 h / 20 °C

3.1: N,N-dimethyl-formamide / 3 h / 20 °C

3.2: 18 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isopropyl alcohol; In N,N-dimethyl-formamide;

Reference yield:

: 23814-12-2
1h-benzotriazole-5-carboxylic acid

: 1246639-64-4
3,5-dichlorobenzyl 4-{2-[(1H-benzotriazole-5-carbonyl)amino]-ethyl}piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 4-methyl-morpholine / N,N-dimethyl-formamide / 18 h / 20 °C

2.1: hydrogenchloride; isopropyl alcohol / 2 h / 20 °C

3.1: N,N-dimethyl-formamide / 3 h / 20 °C

3.2: 18 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isopropyl alcohol; In N,N-dimethyl-formamide;