ethyl (1S,2S,6S,αS)-2-N-benzyl-N-α-methylbenzylamino-6-(ethyloxycarbonylmethyl)cyclohexanecarboxylate

Base Information

Chemical Name:ethyl (1S,2S,6S,αS)-2-N-benzyl-N-α-methylbenzylamino-6-(ethyloxycarbonylmethyl)cyclohexanecarboxylate
CAS No.:852052-20-1
Molecular Formula:C₂₈H₃₇NO₄
Molecular Weight:451.606
Hs Code.:

Synonyms:ethyl (1S,2S,6S,αS)-2-N-benzyl-N-α-methylbenzylamino-6-(ethyloxycarbonylmethyl)cyclohexanecarboxylate

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Chemical Property of ethyl (1S,2S,6S,αS)-2-N-benzyl-N-α-methylbenzylamino-6-(ethyloxycarbonylmethyl)cyclohexanecarboxylate

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Technology Process of ethyl (1S,2S,6S,αS)-2-N-benzyl-N-α-methylbenzylamino-6-(ethyloxycarbonylmethyl)cyclohexanecarboxylate

There total 2 articles about ethyl (1S,2S,6S,αS)-2-N-benzyl-N-α-methylbenzylamino-6-(ethyloxycarbonylmethyl)cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 15898-67-6
(E,E)-nona-2,7-dienedioic acid diethyl ester

: 17480-69-2
(S)-N-benzyl-1-phenylethylamine

: 852052-20-1
ethyl (1S,2S,6S,αS)-2-N-benzyl-N-α-methylbenzylamino-6-(ethyloxycarbonylmethyl)cyclohexanecarboxylate

Guidance literature:: (S)-N-benzyl-1-phenylethylamine; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

(E,E)-nona-2,7-dienedioic acid diethyl ester; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1039/b500223k

Reference yield:

: 111-30-8,29257-65-6,79215-57-9
Glutaraldehyde

: 852052-20-1
ethyl (1S,2S,6S,αS)-2-N-benzyl-N-α-methylbenzylamino-6-(ethyloxycarbonylmethyl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 81 percent / aq. K₂CO₃ / 16 h / 20 °C

2.1: n-BuLi / tetrahydrofuran / 0.5 h / -78 °C

2.2: 82 percent / tetrahydrofuran / 2 h / -78 °C

With n-butyllithium; potassium carbonate; In tetrahydrofuran;
DOI:10.1039/b500223k