3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionic acid ethyl ester

Base Information

• Chemical Name: 3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionic acid ethyl ester
• CAS No.: 125718-84-5
• Molecular Formula: C₂₆H₃₅N₃O₂
• Molecular Weight: 421.583

Synonyms:3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionic acid ethyl ester

Chemical Property of 3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionic acid ethyl ester

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Technology Process of 3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionic acid ethyl ester

There total 5 articles about 3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

benzyl bromide (100-39-0) + 3-{4-[Benzyl-(2-cyano-ethyl)-amino]-butylamino}-propionic acid ethyl ester (125718-88-9) → 3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionic acid ethyl ester (125718-84-5)

Guidance literature:

With potassium fluoride; Celite; In acetonitrile; Heating;

DOI:10.1016/S0040-4039(01)80392-0

Reference yield:

3-(benzylamino)propionitrile (706-03-6) → 3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionic acid ethyl ester (125718-84-5)

Guidance literature:

Multi-step reaction with 4 steps

1: 85.8 percent / KF/celite / acetonitrile / Heating

2: 96 percent / hydrazine / methanol

3: 99 percent

4: 81 percent / KF/celite / acetonitrile / Heating

With potassium fluoride; Celite; hydrazine; In methanol; acetonitrile;

DOI:10.1016/S0040-4039(01)80392-0

Reference yield:

3-[(4-Amino-butyl)-benzyl-amino]-propionitrile (125718-87-8) → 3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionic acid ethyl ester (125718-84-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent

2: 81 percent / KF/celite / acetonitrile / Heating

With potassium fluoride; Celite; In acetonitrile;

DOI:10.1016/S0040-4039(01)80392-0

upstream raw materials:

benzyl bromide

3-{4-[Benzyl-(2-cyano-ethyl)-amino]-butylamino}-propionic acid ethyl ester

3-(benzylamino)propionitrile

3-[(4-Amino-butyl)-benzyl-amino]-propionitrile

Downstream raw materials:

(S)-N¹-(5-{3-[4-(3-Amino-propylamino)-butylamino]-propionylamino}-pentyl)-2-[2-(2,4-dihydroxy-phenyl)-acetylamino]-succinamide; hydrochloride

(S)-N¹-{5-[3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionylamino]-pentyl}-2-[2-(2,4-bis-benzyloxy-phenyl)-acetylamino]-succinamide

((S)-1-{5-[3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionylamino]-pentylcarbamoyl}-2-carbamoyl-ethyl)-carbamic acid tert-butyl ester

{5-[3-(Benzyl-{4-[benzyl-(2-cyano-ethyl)-amino]-butyl}-amino)-propionylamino]-pentyl}-carbamic acid tert-butyl ester

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