Technology Process of 6-hexanoic acid N-hydroxysuccinimide ester
There total 4 articles about 6-hexanoic acid N-hydroxysuccinimide ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicyclohexyl-carbodiimide;
In
dichloromethane;
DOI:10.1021/jm00040a018
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84 percent / NaHCO3 / H2O / 6 h / 0 °C
2: 70 percent / CrO3, H2SO4 / acetone / 0.5 h / 10 - 15 °C
3: 84 percent / dicyclohexylcarbodiimide / CH2Cl2
With
chromium(VI) oxide; sulfuric acid; sodium hydrogencarbonate; dicyclohexyl-carbodiimide;
In
dichloromethane; water; acetone;
DOI:10.1021/jm00040a018
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 70 percent / CrO3, H2SO4 / acetone / 0.5 h / 10 - 15 °C
2: 84 percent / dicyclohexylcarbodiimide / CH2Cl2
With
chromium(VI) oxide; sulfuric acid; dicyclohexyl-carbodiimide;
In
dichloromethane; acetone;
DOI:10.1021/jm00040a018
