4-iodophenyl dimethylcarbamate

Base Information

Chemical Name:4-iodophenyl dimethylcarbamate
CAS No.:84695-01-2
Molecular Formula:C₉H₁₀INO₂
Molecular Weight:291.088
Hs Code.:

Synonyms:4-iodophenyl dimethylcarbamate

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Chemical Property of 4-iodophenyl dimethylcarbamate

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Technology Process of 4-iodophenyl dimethylcarbamate

There total 1 articles about 4-iodophenyl dimethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 540-38-5
p-Iodophenol

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 84695-01-2
4-iodophenyl dimethylcarbamate

Guidance literature:: With potassium carbonate; In acetone; for 2h; Reflux;
DOI:10.1021/acs.orglett.0c00589

Reference yield: 66.0%

: 84695-01-2
4-iodophenyl dimethylcarbamate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: methyl 3-(2-(dimethylcarbamoyloxy)-5-iodophenyl)propanoate

: dimethyl 3,3'-(2-(dimethylcarbamoyloxy)-5-iodo-1,3-phenylene)dipropanoate

Guidance literature:: With silver hexafluoroantimonate; carbonyl(pentamethylcyclopentadienyl)cobalt diiodide; potassium acetate; Trimethylacetic acid; In 1,2-dichloro-ethane; at 100 ℃; for 18h; regioselective reaction; Sealed tube;
DOI:10.1021/acs.orglett.0c00589

Reference yield:

: 84695-01-2
4-iodophenyl dimethylcarbamate

: 4'-formyl-3'-((4-methylphenyl)sulfonamido)-[1,1'-biphenyl]-4-yl dimethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; potassium carbonate / isopropyl alcohol; water / 20 °C

2: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) triflimide; 2-fluoro-5-(trifluoromethyl)aniline; silver trifluoroacetate; trifluoroacetic acid / 1,2-dichloro-ethane / 24 h / 50 °C

With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; 2-fluoro-5-(trifluoromethyl)aniline; palladium diacetate; silver trifluoroacetate; potassium carbonate; trifluoroacetic acid; silver(I) triflimide; In water; 1,2-dichloro-ethane; isopropyl alcohol;
DOI:10.1021/jacs.6b11188