allyl 3-O(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-6-O-(4-methoxyphenol)-α-D-glycopyranoside

Base Information

Chemical Name:allyl 3-O(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-6-O-(4-methoxyphenol)-α-D-glycopyranoside
CAS No.:1343988-82-8
Molecular Formula:C₅₇H₆₂O₁₂
Molecular Weight:939.112
Hs Code.:

Synonyms:allyl 3-O(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-6-O-(4-methoxyphenol)-α-D-glycopyranoside

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Chemical Property of allyl 3-O(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-6-O-(4-methoxyphenol)-α-D-glycopyranoside

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Technology Process of allyl 3-O(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-6-O-(4-methoxyphenol)-α-D-glycopyranoside

There total 12 articles about allyl 3-O(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-6-O-(4-methoxyphenol)-α-D-glycopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1343987-72-3
allyl 3-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-4,6-O-benzylidene-α-D-glucopyranoside

: 150-76-5
4-methoxy-phenol

: 1343988-82-8
allyl 3-O(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-6-O-(4-methoxyphenol)-α-D-glycopyranoside

Guidance literature:: allyl 3-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-4,6-O-benzylidene-α-D-glucopyranoside; 4-methoxy-phenol; With triphenylphosphine; In dichloromethane; at 0 ℃; for 0.666667h;

With diethylazodicarboxylate; In dichloromethane; toluene; at 0 - 20 ℃;

Reference yield:

: 7464-56-4,821794-45-0
1-O-allyl-α-D-glucopyranoside

: 1343988-82-8
allyl 3-O(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-6-O-(4-methoxyphenol)-α-D-glycopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: camphor-10-sulfonic acid / acetonitrile / 20 °C

2.1: pyridine / 4 h / -20 °C

3.1: dichloromethane / 0.17 h / AW-300 molecular sieves

3.2: 0.5 h / 0 °C

4.1: sodium methylate; methanol / tetrahydrofuran / 18 h / 20 °C / AW-300 molecular sieves

5.1: triphenylphosphine / dichloromethane / 0.67 h / 0 °C

5.2: 0 - 20 °C

With pyridine; methanol; sodium methylate; triphenylphosphine; camphor-10-sulfonic acid; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 2280-44-6
D-Glucose

: 1343988-82-8
allyl 3-O(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-6-O-(4-methoxyphenol)-α-D-glycopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetyl chloride / 0 - 40 °C

2.1: camphor-10-sulfonic acid / acetonitrile / 20 °C

3.1: pyridine / 4 h / -20 °C

4.1: dichloromethane / 0.17 h / AW-300 molecular sieves

4.2: 0.5 h / 0 °C

5.1: sodium methylate; methanol / tetrahydrofuran / 18 h / 20 °C / AW-300 molecular sieves

6.1: triphenylphosphine / dichloromethane / 0.67 h / 0 °C

6.2: 0 - 20 °C

With pyridine; methanol; sodium methylate; acetyl chloride; triphenylphosphine; camphor-10-sulfonic acid; In tetrahydrofuran; dichloromethane; acetonitrile;