methyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-3-O-(N-imidazole-1-sulfonyl)-α-D-glucopyranoside

Base Information Edit

Chemical Name:methyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-3-O-(N-imidazole-1-sulfonyl)-α-D-glucopyranoside
CAS No.:79698-60-5
Molecular Formula:C₂₅H₂₇N₃O₉S
Molecular Weight:545.57
Hs Code.:
Mol file:79698-60-5.mol

Synonyms:methyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-3-O-(N-imidazole-1-sulfonyl)-α-D-glucopyranoside

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Chemical Property of methyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-3-O-(N-imidazole-1-sulfonyl)-α-D-glucopyranoside Edit

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Technology Process of methyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-3-O-(N-imidazole-1-sulfonyl)-α-D-glucopyranoside

There total 2 articles about methyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-3-O-(N-imidazole-1-sulfonyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 288-32-4
1H-imidazole

: 60076-41-7
methyl 4,6-O-benzylidene-2-(benzyloxycarbonyl)amino-2-deoxy-α-D-glucopyranoside

: 79698-60-5
methyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-3-O-(N-imidazole-1-sulfonyl)-α-D-glucopyranoside

Guidance literature:: With sulfuryl dichloride; In N,N-dimethyl-formamide; for 1h; Ambient temperature;
DOI:10.1016/0040-4020(96)00586-8

Reference yield:

: 288-32-4
1H-imidazole

: 90-76-6,90-77-7,530-23-4,579-32-8,579-33-9,643-68-5,2596-19-2,6490-68-2,6490-70-6,6490-72-8,6490-73-9,6490-74-0,14196-84-0,14196-86-2,14257-69-3,58381-21-8
glucosamine

: 100-52-7
benzaldehyde

: 79698-60-5
Imidazole-1-sulfonic acid (2R,4aR,6S,7R,8R,8aR)-7-benzyloxycarbonylamino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Guidance literature:: With formic acid; sulfuryl dichloride; Yield given. Multistep reaction; 2.) DMF, -40 deg C; 25 deg C;
DOI:10.1021/ja00410a056