propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-<3,4,6-tri-O-acetyl-2-(chloroacetamido)-2-deoxy-β-D-glucopyranosyl>-β-D-glucopyranoside

Base Information

• Chemical Name: propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-<3,4,6-tri-O-acetyl-2-(chloroacetamido)-2-deoxy-β-D-glucopyranosyl>-β-D-glucopyranoside
• CAS No.: 72894-35-0
• Molecular Formula: C₃₉H₅₁ClN₂O₁₄
• Molecular Weight: 807.292

Synonyms:propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-<3,4,6-tri-O-acetyl-2-(chloroacetamido)-2-deoxy-β-D-glucopyranosyl>-β-D-glucopyranoside

Chemical Property of propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-<3,4,6-tri-O-acetyl-2-(chloroacetamido)-2-deoxy-β-D-glucopyranosyl>-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-<3,4,6-tri-O-acetyl-2-(chloroacetamido)-2-deoxy-β-D-glucopyranosyl>-β-D-glucopyranoside

There total 3 articles about propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-<3,4,6-tri-O-acetyl-2-(chloroacetamido)-2-deoxy-β-D-glucopyranosyl>-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside (72366-33-7) + 1,3,4,6-tetra-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranoside (68499-56-9) → propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-<3,4,6-tri-O-acetyl-2-(chloroacetamido)-2-deoxy-β-D-glucopyranosyl>-β-D-glucopyranoside (72894-35-0)

Guidance literature:

With calcium sulfate; iron(III) chloride; tetramethylurea; In dichloromethane; at 35 ℃;

DOI:10.1016/0008-6215(85)85205-8

Reference yield:

tetra-acetyl glucosamine (17460-45-6,23707-23-5,23739-93-7,23743-51-3,26108-75-8,59042-16-9,124516-07-0,124580-56-9) → propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-<3,4,6-tri-O-acetyl-2-(chloroacetamido)-2-deoxy-β-D-glucopyranosyl>-β-D-glucopyranoside (72894-35-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / 2,6-dimethylpyridine / CHCl₃ / 1 h / -10 - 0 °C

2: 60 percent / FeCl₃, CaSO₄, tetramethylurea / CH₂Cl₂ / 35 °C

With 2,6-dimethylpyridine; calcium sulfate; iron(III) chloride; tetramethylurea; In dichloromethane; chloroform;

DOI:10.1016/0008-6215(85)85205-8

Reference yield:

→ propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-<3,4,6-tri-O-acetyl-2-(chloroacetamido)-2-deoxy-β-D-glucopyranosyl>-β-D-glucopyranoside (72894-35-0)

Guidance literature:

Tetraacetat 1d, Alkohol 3, FeCl3;

DOI:10.1016/S0008-6215(00)83963-4

upstream raw materials:

propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

1,3,4,6-tetra-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranoside

tetra-acetyl glucosamine

Downstream raw materials:

propyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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