diphenyl (2,3,4-tri-O-benzyl-6-O-diphenoxyphosphoryl-β-D-fructofuranosyl)phosphonate

Base Information

Chemical Name:diphenyl (2,3,4-tri-O-benzyl-6-O-diphenoxyphosphoryl-β-D-fructofuranosyl)phosphonate
CAS No.:117325-35-6
Molecular Formula:C₅₁H₄₈O₁₁P₂
Molecular Weight:898.883
Hs Code.:

Synonyms:diphenyl (2,3,4-tri-O-benzyl-6-O-diphenoxyphosphoryl-β-D-fructofuranosyl)phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyl (2,3,4-tri-O-benzyl-6-O-diphenoxyphosphoryl-β-D-fructofuranosyl)phosphonate

Chemical Property:

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Technology Process of diphenyl (2,3,4-tri-O-benzyl-6-O-diphenoxyphosphoryl-β-D-fructofuranosyl)phosphonate

There total 4 articles about diphenyl (2,3,4-tri-O-benzyl-6-O-diphenoxyphosphoryl-β-D-fructofuranosyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101-02-0
triphenyl phosphite

: 117325-35-6
diphenyl (2,3,4-tri-O-benzyl-6-O-diphenoxyphosphoryl-β-D-fructofuranosyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / Ambient temperature

2: 67 percent / boron trifluoride etherate / 1.) from -40 deg C to 0 deg C, 3 h; 2.) 3 h, 0 deg C

3: 1.) sodium 3-nitrophenoxide / 1.) MeOH, 3 h, reflux; 2.) pyridine, 30 min, 0 deg C

With trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; sodium 3-nitrophenoxide; In dichloromethane;
DOI:10.1016/0008-6215(88)85080-8

Reference yield:

: 92691-81-1
2-O-acetyl-1,3,4,6-tetra-O-benzyl-α,β-D-fructofuranose

: 117325-35-6
diphenyl (2,3,4-tri-O-benzyl-6-O-diphenoxyphosphoryl-β-D-fructofuranosyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / Ambient temperature

2: 67 percent / boron trifluoride etherate / 1.) from -40 deg C to 0 deg C, 3 h; 2.) 3 h, 0 deg C

3: 1.) sodium 3-nitrophenoxide / 1.) MeOH, 3 h, reflux; 2.) pyridine, 30 min, 0 deg C

With trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; sodium 3-nitrophenoxide; In dichloromethane;
DOI:10.1016/0008-6215(88)85080-8

Reference yield:

: 117325-29-8
diphenyl (1,3,4,6-tetra-O-benzyl-β-D-fructofuranosyl)phosphonate

: 117325-35-6
diphenyl (2,3,4-tri-O-benzyl-6-O-diphenoxyphosphoryl-β-D-fructofuranosyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / boron trifluoride etherate / 1.) from -40 deg C to 0 deg C, 3 h; 2.) 3 h, 0 deg C

2: 1.) sodium 3-nitrophenoxide / 1.) MeOH, 3 h, reflux; 2.) pyridine, 30 min, 0 deg C

boron trifluoride diethyl etherate; sodium 3-nitrophenoxide;
DOI:10.1016/0008-6215(88)85080-8