ethyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-thio-α-D-arabinofuranoside

Base Information

Chemical Name:ethyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-thio-α-D-arabinofuranoside
CAS No.:628686-37-3
Molecular Formula:C₂₆H₄₄O₆SSi₂
Molecular Weight:540.869
Hs Code.:

Synonyms:ethyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-thio-α-D-arabinofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-thio-α-D-arabinofuranoside

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Technology Process of ethyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-thio-α-D-arabinofuranoside

There total 1 articles about ethyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-thio-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 98-88-4
benzoyl chloride

: 243642-91-3
ethyl 3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-thio-α-D-arabinofuranoside

: 628686-37-3
ethyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-thio-α-D-arabinofuranoside

Guidance literature:: With pyridine; at 20 ℃; for 3h;
DOI:10.1002/ejoc.200300303

Reference yield: 87.0%

: 282107-63-5
8-methoxycarbonyloctyl 2-O-benzoyl-3-O-benzyl-α-D-arabinofuranoside

: 628686-37-3
ethyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-thio-α-D-arabinofuranoside

: 628686-54-4
8-(methoxycarbonyl)octyl 2-O-benzoyl-5-O-[2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)-α-D-arabinofuranosyl]-3-O-benzyl-α-D-arabinofuranoside

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1002/ejoc.200300303

Reference yield: 81.0%

: 628686-37-3
ethyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-thio-α-D-arabinofuranoside

: 628686-39-5
8-(methoxycarbonyl)octyl 2-O-benzoyl-5-O-(2-O-benzoyl-3-O-benzyl-α-D-arabinofuranosyl)-3-O-benzyl-α-D-arabinofuranoside

: 628686-45-3
8-(methoxycarbonyl)octyl 2-O-benzoyl-5-O-{2-O-benzoyl-5-O-[2-O-benzoyl-3,5-di-O-(1,1,3,3-tetra-isopropyldisiloxan-1,3-diyl)-α-D-arabinofuranosyl]-3-O-benzyl-α-D-arabinofuranosyl}-3-O-benzyl-α-D-arabinofuranoside

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -15 ℃; for 1h;
DOI:10.1002/ejoc.200300303