benzhydryl (S)-2-(2,4-dinitrophenylsulfonamido)-3-hydroxy-3-methylbutanoate

Base Information

Chemical Name:benzhydryl (S)-2-(2,4-dinitrophenylsulfonamido)-3-hydroxy-3-methylbutanoate
CAS No.:1275621-82-3
Molecular Formula:C₂₄H₂₃N₃O₉S
Molecular Weight:529.527
Hs Code.:

Synonyms:benzhydryl (S)-2-(2,4-dinitrophenylsulfonamido)-3-hydroxy-3-methylbutanoate

Suppliers and Price of benzhydryl (S)-2-(2,4-dinitrophenylsulfonamido)-3-hydroxy-3-methylbutanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzhydryl (S)-2-(2,4-dinitrophenylsulfonamido)-3-hydroxy-3-methylbutanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzhydryl (S)-2-(2,4-dinitrophenylsulfonamido)-3-hydroxy-3-methylbutanoate

There total 4 articles about benzhydryl (S)-2-(2,4-dinitrophenylsulfonamido)-3-hydroxy-3-methylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 473545-40-3
tert-butyl N-[(1R)-2-hydroxy-1-(hydroxymethyl)-2-methylpropyl]carbamate

: 1275621-82-3
benzhydryl (S)-2-(2,4-dinitrophenylsulfonamido)-3-hydroxy-3-methylbutanoate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / acetonitrile / 0 - 20 °C / pH 6.4 / aq. phosphate buffer

2: dichloromethane / 0 - 20 °C

3: hydrogenchloride / methanol / 1 h / -10 °C

4: sodium carbonate / tetrahydrofuran; water / 0 - 20 °C

With hydrogenchloride; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; sodium carbonate; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1002/anie.201004646

Reference yield:

: 1275621-80-1
benzhydryl (S)-2-(tert-butoxycarbonylamino)-3-hydroxy-3-methylbutanoate

: 1275621-82-3
benzhydryl (S)-2-(2,4-dinitrophenylsulfonamido)-3-hydroxy-3-methylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol / 1 h / -10 °C

2: sodium carbonate / tetrahydrofuran; water / 0 - 20 °C

With hydrogenchloride; sodium carbonate; In tetrahydrofuran; methanol; water;
DOI:10.1002/anie.201004646

Reference yield:

: 288159-36-4
tert-butyl (4R)-4-(1-hydroxy-1-methylethyl)-2,2-dimethyl-1,3-oxazolidine-3-carboxylate

: 1275621-82-3
benzhydryl (S)-2-(2,4-dinitrophenylsulfonamido)-3-hydroxy-3-methylbutanoate

Guidance literature:: Multi-step reaction with 5 steps

1: methanol; pyridinium p-toluenesulfonate / 4 h / 20 °C

2: sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / acetonitrile / 0 - 20 °C / pH 6.4 / aq. phosphate buffer

3: dichloromethane / 0 - 20 °C

4: hydrogenchloride / methanol / 1 h / -10 °C

5: sodium carbonate / tetrahydrofuran; water / 0 - 20 °C

With hydrogenchloride; methanol; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; pyridinium p-toluenesulfonate; sodium carbonate; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1002/anie.201004646