2,3-di-O-benzoyl-4-deoxy-4-fluoro-β-D-xylopyranosylazide

Base Information

Chemical Name:2,3-di-O-benzoyl-4-deoxy-4-fluoro-β-D-xylopyranosylazide
CAS No.:1092390-48-1
Molecular Formula:C₁₉H₁₆FN₃O₅
Molecular Weight:385.352
Hs Code.:

Synonyms:2,3-di-O-benzoyl-4-deoxy-4-fluoro-β-D-xylopyranosylazide

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Chemical Property of 2,3-di-O-benzoyl-4-deoxy-4-fluoro-β-D-xylopyranosylazide

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Technology Process of 2,3-di-O-benzoyl-4-deoxy-4-fluoro-β-D-xylopyranosylazide

There total 3 articles about 2,3-di-O-benzoyl-4-deoxy-4-fluoro-β-D-xylopyranosylazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 943621-49-6
1,2,3-tri-O-benzoyl-4-deoxy-4-fluoro-α-D-xylopyranose

: 1092390-48-1
2,3-di-O-benzoyl-4-deoxy-4-fluoro-β-D-xylopyranosylazide

Guidance literature:: With trimethylsilylazide; tin(IV) chloride; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/j.bmcl.2010.10.085

Reference yield:

: 4-hydroxy-1-azido-2,3,4-tribenzoyl-α-L-arabinose

: 1092390-48-1
2,3-di-O-benzoyl-4-deoxy-4-fluoro-β-D-xylopyranosylazide

Guidance literature:: With diethylamino-sulfur trifluoride; at -40 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.molpharmaceut.0c00839

Reference yield:

: 51970-32-2
β-L-arabinopyranosyl azide

: 98-88-4
benzoyl chloride

: 1092390-48-1
2,3-di-O-benzoyl-4-deoxy-4-fluoro-β-D-xylopyranosylazide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 16 h / -40 - 20 °C / Inert atmosphere

2: diethylamino-sulfur trifluoride / 16 h / -40 - 20 °C / Inert atmosphere

With pyridine; diethylamino-sulfur trifluoride;
DOI:10.1021/acs.molpharmaceut.0c00839