[5,15-bis(3',5'-di-tert-butylphenyl)-10-(amino)porphyrinato]zinc(II)

Base Information

Chemical Name:[5,15-bis(3',5'-di-tert-butylphenyl)-10-(amino)porphyrinato]zinc(II)
CAS No.:438457-42-2
Molecular Formula:C₄₈H₅₃N₅Zn
Molecular Weight:765.372
Hs Code.:

Synonyms:[5,15-bis(3',5'-di-tert-butylphenyl)-10-(amino)porphyrinato]zinc(II)

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Chemical Property of [5,15-bis(3',5'-di-tert-butylphenyl)-10-(amino)porphyrinato]zinc(II)

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Technology Process of [5,15-bis(3',5'-di-tert-butylphenyl)-10-(amino)porphyrinato]zinc(II)

There total 1 articles about [5,15-bis(3',5'-di-tert-butylphenyl)-10-(amino)porphyrinato]zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 13755-29-8
sodium tetrafluoroborate

: 187387-21-9
[5,15-bis(3',5'-di-tert-butylphenyl)-10-(nitro)porphyrinato]zinc(II)

: 438457-42-2
[5,15-bis(3',5'-di-tert-butylphenyl)-10-(amino)porphyrinato]zinc(II)

Guidance literature:: With Pd/C; In methanol; dichloromethane; Pd on carbon was added to soln. of Zn complex in CH2Cl2/methanol; mixt. was degassed; NaBF4 added over 20 min; mixt. was stirred at room temp. for 1.5 h; filtered; filtrate washed (water); org. phase evapd.; recrystd. (CH2Cl2/methanol);
DOI:10.1039/b109915a

Reference yield: 68.0%

: 438457-42-2
[5,15-bis(3',5'-di-tert-butylphenyl)-10-(amino)porphyrinato]zinc(II)

: 100-52-7
benzaldehyde

: [5,15-bis(3',5'-di-tert-butylphenyl)-10-(phenylmethylideneamino)porphyrinato]zinc(II)

Guidance literature:: In toluene; (Ar); toluene and C6H5CHO were added to Zn complex and Amberlyst 15; mixt. was refluxed for 3 h over Soxhlet app. with mol. sieves; filtered; chromd. (petroleum ether/EtOAc/pyridine, 10/1/0.1); recrystd. (CHCl3/methanol);
DOI:10.1039/b109915a

Reference yield: 52.0%

: 4664-08-8
cinchomeronic anhydride

: 438457-42-2
[5,15-bis(3',5'-di-tert-butylphenyl)-10-(amino)porphyrinato]zinc(II)

: 897937-40-5
Zn(II) 10-cinchomeronimide-5,15-bis(3,5-di-tert-butylphenyl)porphyrin

Guidance literature:: In pyridine; soln. Zn complex and cinchomeronic anhydride in pyridine was heated under reflux for 14 h; solvent was removed, chromy. on silica (THF-hexane);
DOI:10.1021/ja0611137