4-Phenyl-2-butanone diethyldithioacetal

Base Information

• Chemical Name: 4-Phenyl-2-butanone diethyldithioacetal
• CAS No.: 108164-52-9
• Molecular Formula: C₁₄H₂₂S₂
• Molecular Weight: 254.461

Synonyms:4-Phenyl-2-butanone diethyldithioacetal

Chemical Property of 4-Phenyl-2-butanone diethyldithioacetal

Chemical Property:

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Technology Process of 4-Phenyl-2-butanone diethyldithioacetal

There total 1 articles about 4-Phenyl-2-butanone diethyldithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-Phenyl-2-butanone (2550-26-7) + ethanethiol (75-08-1) → 4-Phenyl-2-butanone diethyldithioacetal (108164-52-9)

Guidance literature:

With hafnium(IV) trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jo8021988

Reference yield: 96.0%

4-Phenyl-2-butanone diethyldithioacetal (108164-52-9) → 4-Phenyl-2-butanone (2550-26-7)

Guidance literature:

With gallium(III) trichloride; In dichloromethane; water; for 0.25h; Ambient temperature;

Reference yield: 82.0%

allyltributylstanane (24850-33-7) + 4-Phenyl-2-butanone diethyldithioacetal (108164-52-9) → (3-Ethylsulfanyl-3-methyl-hex-5-enyl)-benzene (130839-82-6)

Guidance literature:

With gallium(III) trichloride; In dichloromethane; at -45 ℃; for 3h;

DOI:10.1246/cl.1990.1097

upstream raw materials:

4-Phenyl-2-butanone

ethanethiol

Downstream raw materials:

(3-Ethylsulfanyl-3-methyl-hex-5-enyl)-benzene

4-Phenyl-2-butanone

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