Technology Process of C68H105N15O7S
There total 12 articles about C68H105N15O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C50H77N15O;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 20 - 26 ℃;
Inert atmosphere;
C18H29BrO6S;
In
tetrahydrofuran; mineral oil;
at 20 - 26 ℃;
for 48h;
Reagent/catalyst;
Solvent;
Time;
Inert atmosphere;
DOI:10.1016/j.tet.2013.01.070
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dimethylsulfide borane complex / tetrahydrofuran / 20 - 26 °C / Inert atmosphere
2.1: acetic acid / 48 h / Reflux
3.1: dimethylsulfide borane complex / tetrahydrofuran / 20 - 26 °C / Inert atmosphere
4.1: methanol / 48 h / Reflux
5.1: sodium hydride / tetrahydrofuran; mineral oil / 20 - 26 °C / Inert atmosphere
5.2: 48 h / 20 - 26 °C / Inert atmosphere
With
dimethylsulfide borane complex; sodium hydride; acetic acid;
In
tetrahydrofuran; methanol; mineral oil;
2.1: |Michael Addition / 4.1: |Michael Addition;
DOI:10.1016/j.tet.2013.01.070
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid / 48 h / Reflux
2.1: dimethylsulfide borane complex / tetrahydrofuran / 20 - 26 °C / Inert atmosphere
3.1: methanol / 48 h / Reflux
4.1: sodium hydride / tetrahydrofuran; mineral oil / 20 - 26 °C / Inert atmosphere
4.2: 48 h / 20 - 26 °C / Inert atmosphere
With
dimethylsulfide borane complex; sodium hydride; acetic acid;
In
tetrahydrofuran; methanol; mineral oil;
1.1: |Michael Addition / 3.1: |Michael Addition;
DOI:10.1016/j.tet.2013.01.070