Technology Process of C35H42O4Si
There total 5 articles about C35H42O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydride;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
at 0 ℃;
Yield given;
DOI:10.1021/ja00354a060
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) NaH / 1.) THF, 25 deg C
2: 92 percent / toluene / 15 h / 68 °C
3: 96 percent / NaBH4, CeCl3 / toluene; methanol / -78 °C
4: collidine / toluene / -100 °C
5: KH / tetrahydrofuran; hexamethylphosphoric acid triamide / 0 °C
With
2,3,5-trimethyl-pyridine; sodium tetrahydroborate; cerium(III) chloride; potassium hydride; sodium hydride;
In
tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; toluene;
DOI:10.1021/ja00354a060
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 92 percent / toluene / 15 h / 68 °C
2: 96 percent / NaBH4, CeCl3 / toluene; methanol / -78 °C
3: collidine / toluene / -100 °C
4: KH / tetrahydrofuran; hexamethylphosphoric acid triamide / 0 °C
With
2,3,5-trimethyl-pyridine; sodium tetrahydroborate; cerium(III) chloride; potassium hydride;
In
tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; toluene;
DOI:10.1021/ja00354a060