ethyl 2,3,4-tri-O-benzyl-6-O-trityl-β-D-glucopyranosyl-(1->2)-2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside

Base Information

• Chemical Name: ethyl 2,3,4-tri-O-benzyl-6-O-trityl-β-D-glucopyranosyl-(1->2)-2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside
• CAS No.: 1048014-65-8
• Molecular Formula: C₉₀H₉₄O₁₄S
• Molecular Weight: 1431.79

Synonyms:ethyl 2,3,4-tri-O-benzyl-6-O-trityl-β-D-glucopyranosyl-(1->2)-2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside

Chemical Property of ethyl 2,3,4-tri-O-benzyl-6-O-trityl-β-D-glucopyranosyl-(1->2)-2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside

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Technology Process of ethyl 2,3,4-tri-O-benzyl-6-O-trityl-β-D-glucopyranosyl-(1->2)-2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside

There total 1 articles about ethyl 2,3,4-tri-O-benzyl-6-O-trityl-β-D-glucopyranosyl-(1->2)-2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

ethyl 6-O-trityl-β-D-glucopyranosyl-(1->2)-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside (1048014-64-7) + benzyl bromide (100-39-0) → ethyl 2,3,4-tri-O-benzyl-6-O-trityl-β-D-glucopyranosyl-(1->2)-2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside (1048014-65-8)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.carres.2007.11.026

Reference yield: 72.0%

ethyl 2,3,4-tri-O-benzyl-6-O-trityl-β-D-glucopyranosyl-(1->2)-2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside (1048014-65-8) → ethyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside (1048014-68-1)

Guidance literature:

With toluene-4-sulfonic acid; In chloroform; water; at 20 ℃;

DOI:10.1016/j.carres.2007.11.026

upstream raw materials:

ethyl 6-O-trityl-β-D-glucopyranosyl-(1->2)-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside

benzyl bromide

Downstream raw materials:

ethyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-1-thio-α-D-mannopyranoside

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