(7S,8S)-7,8-bis((benzyloxy)methyl)-1,14-dichloro-3,6,9,12-tetraoxatetradecane

Base Information

Chemical Name:(7S,8S)-7,8-bis((benzyloxy)methyl)-1,14-dichloro-3,6,9,12-tetraoxatetradecane
CAS No.:88454-97-1
Molecular Formula:C₂₆H₃₆Cl₂O₆
Molecular Weight:515.474
Hs Code.:

Synonyms:(7S,8S)-7,8-bis((benzyloxy)methyl)-1,14-dichloro-3,6,9,12-tetraoxatetradecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (7S,8S)-7,8-bis((benzyloxy)methyl)-1,14-dichloro-3,6,9,12-tetraoxatetradecane

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Technology Process of (7S,8S)-7,8-bis((benzyloxy)methyl)-1,14-dichloro-3,6,9,12-tetraoxatetradecane

There total 5 articles about (7S,8S)-7,8-bis((benzyloxy)methyl)-1,14-dichloro-3,6,9,12-tetraoxatetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 17401-06-8
(2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol

: 111-44-4
3-oxa-1,5-dichloropentane

: 88454-97-1
(7S,8S)-7,8-bis((benzyloxy)methyl)-1,14-dichloro-3,6,9,12-tetraoxatetradecane

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; at 5 - 20 ℃;
DOI:10.1016/S0957-4166(01)00309-3

Reference yield: 62.0%

: 88454-96-0
2-(2-{(1S,2S)-3-Benzyloxy-1-benzyloxymethyl-2-[2-(2-hydroxy-ethoxy)-ethoxy]-propoxy}-ethoxy)-ethanol

: 88454-97-1
(7S,8S)-7,8-bis((benzyloxy)methyl)-1,14-dichloro-3,6,9,12-tetraoxatetradecane

Guidance literature:: With pyridine; thionyl chloride; In benzene; for 14h; Heating;
DOI:10.1021/jo00179a004

Reference yield:

: 88454-94-8,135821-34-0
1,4-Di-O-benzyl-2,3-bis-O-<2-<2-(2-tetrahydropyranyloxy)ethoxy>ethyl>-L-threitol

: 88454-97-1
(7S,8S)-7,8-bis((benzyloxy)methyl)-1,14-dichloro-3,6,9,12-tetraoxatetradecane

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / 5percent HCl / methanol / 2 h / Heating

2: 62 percent / SOCl₂, pyridine / benzene / 14 h / Heating

With pyridine; hydrogenchloride; thionyl chloride; In methanol; benzene;
DOI:10.1021/jo00179a004