C₅₂H₆₉NO₃Si₂

Base Information

Chemical Name:C₅₂H₆₉NO₃Si₂
CAS No.:1404213-31-5
Molecular Formula:C₅₂H₆₉NO₃Si₂
Molecular Weight:812.296
Hs Code.:

C<sub>52</sub>H<sub>69</sub>NO<sub>3</sub>Si<sub>2</sub>

Synonyms:C₅₂H₆₉NO₃Si₂

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Chemical Property of C₅₂H₆₉NO₃Si₂

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Technology Process of C₅₂H₆₉NO₃Si₂

There total 6 articles about C₅₂H₆₉NO₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 149505-94-2
tert-butyl (4-hydroxybenzyl)carbamate

: 1404213-31-5
C₅₂H₆₉NO₃Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium chlorite; sodium iodide / methanol; water

1.2: 20 °C

2.1: potassium carbonate / acetone / Inert atmosphere; Reflux

3.1: trifluoroacetic acid / dichloromethane / 2 h

3.2: 20 °C / Inert atmosphere

4.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: sodium iodide; potassium carbonate / acetone / Reflux

6.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

7.1: potassium hydroxide / methanol; tetrahydrofuran / 1 h

7.2: Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; copper(l) iodide; boron tribromide; potassium carbonate; triethylamine; trifluoroacetic acid; sodium iodide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetone; 6.1: |Sonogashira Cross-Coupling / 7.2: |Sonogashira Cross-Coupling;
DOI:10.1002/ejoc.201200655

Reference yield:

: 1404213-29-1
C₂₂H₃₅I₂NO₃

: 1404213-31-5
C₅₂H₆₉NO₃Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: potassium hydroxide / methanol; tetrahydrofuran / 1 h

2.2: Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; 1.1: |Sonogashira Cross-Coupling / 2.2: |Sonogashira Cross-Coupling;
DOI:10.1002/ejoc.201200655

Reference yield:

: 1404213-20-2
C₂₀H₃₁I₂NO₂

: 1404213-31-5
C₅₂H₆₉NO₃Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

2.1: sodium iodide; potassium carbonate / acetone / Reflux

3.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

4.1: potassium hydroxide / methanol; tetrahydrofuran / 1 h

4.2: Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; boron tribromide; potassium carbonate; triethylamine; sodium iodide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; acetone; 3.1: |Sonogashira Cross-Coupling / 4.2: |Sonogashira Cross-Coupling;
DOI:10.1002/ejoc.201200655