Technology Process of C20H15ClF2N2O6S
There total 7 articles about C20H15ClF2N2O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
formic acid; dihydrogen peroxide;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: benzyl chloride / acetone / 0.25 h / Reflux
1.2: 1 h
2.1: methanol / 0 °C / Reflux
3.1: 4-methyl-morpholine / dichloromethane / -5 - 20 °C / Inert atmosphere
4.1: potassium carbonate / N,N-dimethyl-formamide / 0.75 h / 0 - 20 °C
5.1: sodium hydroxide; water / 1,4-dioxane / 1.5 h / 20 °C
6.1: N-chloro-succinimide; dichloro-acetic acid / 1,2-dichloro-ethane / 3 h / 65 °C / Inert atmosphere
7.1: formic acid; dihydrogen peroxide / 20 °C
With
4-methyl-morpholine; dichloro-acetic acid; N-chloro-succinimide; formic acid; water; dihydrogen peroxide; potassium carbonate; benzyl chloride; sodium hydroxide;
In
1,4-dioxane; methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: methanol / 0 °C / Reflux
2: 4-methyl-morpholine / dichloromethane / -5 - 20 °C / Inert atmosphere
3: potassium carbonate / N,N-dimethyl-formamide / 0.75 h / 0 - 20 °C
4: sodium hydroxide; water / 1,4-dioxane / 1.5 h / 20 °C
5: N-chloro-succinimide; dichloro-acetic acid / 1,2-dichloro-ethane / 3 h / 65 °C / Inert atmosphere
6: formic acid; dihydrogen peroxide / 20 °C
With
4-methyl-morpholine; dichloro-acetic acid; N-chloro-succinimide; formic acid; water; dihydrogen peroxide; potassium carbonate; sodium hydroxide;
In
1,4-dioxane; methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;