C₂₆H₃₁ClN₄O₄S₂

Base Information

Chemical Name:C₂₆H₃₁ClN₄O₄S₂
CAS No.:1027587-64-9
Molecular Formula:C₂₆H₃₁ClN₄O₄S₂
Molecular Weight:563.142
Hs Code.:

C<sub>26</sub>H<sub>31</sub>ClN<sub>4</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:C₂₆H₃₁ClN₄O₄S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₃₁ClN₄O₄S₂

Chemical Property:

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Technology Process of C₂₆H₃₁ClN₄O₄S₂

There total 13 articles about C₂₆H₃₁ClN₄O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144628-52-4
2-butyl-4-(methylthio)-1-[[2'-((((propylamino)-carbonyl)-amino)-sulfonyl)-(1,1'-biphenyl)-4-yl]-methyl]-1H-imidazole-5-carboxylic acid

: 1027587-64-9
C₂₆H₃₁ClN₄O₄S₂

Guidance literature:: With thionyl chloride; In toluene; 1.) RT, 1 h, 2.) 55 deg C, overnight;
DOI:10.1021/jm00013a013

Reference yield:

: 5720-05-8
4-methylphenylboronic acid

: 1027587-64-9
C₂₆H₃₁ClN₄O₄S₂

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / aq. Na₂CO₃, triphenylphosphine, palladium acetate / ethanol; toluene / 4 h / Heating

2: 64 percent / N-bromosuccinimide, benzoyl peroxide / chlorobenzene / 1 h / 120 °C

3: K₂CO₃ / dimethylformamide / 45 h / 20 - 25 °C

4: 81 percent / conc. HCl / ethanol / 2 h / Heating

5: 87 percent / K₂CO₃ / acetone / 2 h / Heating

6: 80 percent / 2N NaOH / ethanol / 24 h / Ambient temperature

7: thionyl chloride / toluene / 1.) RT, 1 h, 2.) 55 deg C, overnight

With hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; thionyl chloride; Perbenzoic acid; palladium diacetate; sodium carbonate; potassium carbonate; triphenylphosphine; In ethanol; N,N-dimethyl-formamide; chlorobenzene; acetone; toluene;
DOI:10.1021/jm00013a013

Reference yield:

: 92748-09-9
2-bromobenzene-1-sulfonamide

: 1027587-64-9
C₂₆H₃₁ClN₄O₄S₂

Guidance literature:: Multi-step reaction with 8 steps

1: 98 percent / dimethylformamide / 2 h / Ambient temperature

2: 93 percent / aq. Na₂CO₃, triphenylphosphine, palladium acetate / ethanol; toluene / 4 h / Heating

3: 64 percent / N-bromosuccinimide, benzoyl peroxide / chlorobenzene / 1 h / 120 °C

4: K₂CO₃ / dimethylformamide / 45 h / 20 - 25 °C

5: 81 percent / conc. HCl / ethanol / 2 h / Heating

6: 87 percent / K₂CO₃ / acetone / 2 h / Heating

7: 80 percent / 2N NaOH / ethanol / 24 h / Ambient temperature

8: thionyl chloride / toluene / 1.) RT, 1 h, 2.) 55 deg C, overnight

With hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; thionyl chloride; Perbenzoic acid; palladium diacetate; sodium carbonate; potassium carbonate; triphenylphosphine; In ethanol; N,N-dimethyl-formamide; chlorobenzene; acetone; toluene;
DOI:10.1021/jm00013a013