1,3-dibenzylazepane

Base Information

Chemical Name:1,3-dibenzylazepane
CAS No.:1264184-64-6
Molecular Formula:C₂₀H₂₅N
Molecular Weight:279.425
Hs Code.:

Synonyms:1,3-dibenzylazepane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-dibenzylazepane

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Technology Process of 1,3-dibenzylazepane

There total 2 articles about 1,3-dibenzylazepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 20422-13-3
1-benzylazepane

: 100-52-7
benzaldehyde

: 1264184-64-6
1,3-dibenzylazepane

Guidance literature:: 1-benzylazepane; benzaldehyde; With C₂₆H₃₂ClO₃PRuS; (1S)-10-camphorsulfonic acid; In toluene; at 140 ℃; for 16h; Inert atmosphere;

With formic acid; In toluene; at 140 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja203875d

Reference yield: 68.0%

: 111-49-9
hexamethylene imine

: 100-51-6,185532-71-2
benzyl alcohol

: 1264184-64-6
1,3-dibenzylazepane

Guidance literature:: hexamethylene imine; With (1S)-10-camphorsulfonic acid; In toluene; for 0.0166667h; Inert atmosphere;

benzyl alcohol; With [Ru(p-cymene)(k⁽²⁾-o-tBuPPBS)Cl]; In toluene; at 150 ℃; for 16h; regioselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201000546