(S)-benzyl [1-(tert-butyldimethylsilanyloxymethyl)-3-methanesulfinylpropyl]carbamate

Base Information

Chemical Name:(S)-benzyl [1-(tert-butyldimethylsilanyloxymethyl)-3-methanesulfinylpropyl]carbamate
CAS No.:672964-45-3
Molecular Formula:C₁₉H₃₃NO₄SSi
Molecular Weight:399.627
Hs Code.:

Synonyms:(S)-benzyl [1-(tert-butyldimethylsilanyloxymethyl)-3-methanesulfinylpropyl]carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-benzyl [1-(tert-butyldimethylsilanyloxymethyl)-3-methanesulfinylpropyl]carbamate

Chemical Property:

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Technology Process of (S)-benzyl [1-(tert-butyldimethylsilanyloxymethyl)-3-methanesulfinylpropyl]carbamate

There total 4 articles about (S)-benzyl [1-(tert-butyldimethylsilanyloxymethyl)-3-methanesulfinylpropyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [1-(tert-butyl-dimethyl-silanyloxymethyl)-3-methylsulfanyl-propyl]-carbamic acid benzyl ester

: 672964-45-3
(S)-benzyl [1-(tert-butyldimethylsilanyloxymethyl)-3-methanesulfinylpropyl]carbamate

Guidance literature:: With sodium periodate; In methanol; at 20 ℃; for 2h;
DOI:10.1002/chem.200305421

Reference yield:

: 63-68-3,26062-47-5,58576-49-1
L-methionine

: 672964-45-3
(S)-benzyl [1-(tert-butyldimethylsilanyloxymethyl)-3-methanesulfinylpropyl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / LiAlH₄ / tetrahydrofuran / Heating

2: aq. KHCO₃ / ethyl acetate / 3.5 h / 0 - 20 °C

3: imidazole / CH₂Cl₂ / 0 - 20 °C

4: 38.04 g / aq. NaIO₄ / methanol / 2 h / 20 °C

With 1H-imidazole; sodium periodate; lithium aluminium tetrahydride; potassium hydrogencarbonate; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1002/chem.200305421

Reference yield:

: 2899-37-8
(S)-methioninol

: 672964-45-3
(S)-benzyl [1-(tert-butyldimethylsilanyloxymethyl)-3-methanesulfinylpropyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: aq. KHCO₃ / ethyl acetate / 3.5 h / 0 - 20 °C

2: imidazole / CH₂Cl₂ / 0 - 20 °C

3: 38.04 g / aq. NaIO₄ / methanol / 2 h / 20 °C

With 1H-imidazole; sodium periodate; potassium hydrogencarbonate; In methanol; dichloromethane; ethyl acetate;
DOI:10.1002/chem.200305421