cyclohexyl-{2-[3-(2-hydroxy-ethyl)-phenyl]-ethyl}-carbamic acid tert-butyl ester

Base Information

Chemical Name:cyclohexyl-{2-[3-(2-hydroxy-ethyl)-phenyl]-ethyl}-carbamic acid tert-butyl ester
CAS No.:950503-34-1
Molecular Formula:C₂₁H₃₃NO₃
Molecular Weight:347.498
Hs Code.:

Synonyms:cyclohexyl-{2-[3-(2-hydroxy-ethyl)-phenyl]-ethyl}-carbamic acid tert-butyl ester

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Chemical Property of cyclohexyl-{2-[3-(2-hydroxy-ethyl)-phenyl]-ethyl}-carbamic acid tert-butyl ester

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Technology Process of cyclohexyl-{2-[3-(2-hydroxy-ethyl)-phenyl]-ethyl}-carbamic acid tert-butyl ester

There total 4 articles about cyclohexyl-{2-[3-(2-hydroxy-ethyl)-phenyl]-ethyl}-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 950503-33-0
2-[3-(2-cyclohexylamino-ethyl)-phenyl]-ethanol

: 24424-99-5
di-tert-butyl dicarbonate

: 950503-34-1
cyclohexyl-{2-[3-(2-hydroxy-ethyl)-phenyl]-ethyl}-carbamic acid tert-butyl ester

Guidance literature:: In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 950503-32-9
(3-cyclohexylcarbamoylmethyl-phenyl)-acetic acid

: 950503-34-1
cyclohexyl-{2-[3-(2-hydroxy-ethyl)-phenyl]-ethyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfide borane complex / dichloromethane / 2 h / 20 °C / Heating / reflux

2: dichloromethane / 2 h / 20 °C

With dimethylsulfide borane complex; In dichloromethane;

Reference yield:

: 19806-17-8
1,3-benzenediacetic acid

: 950503-34-1
cyclohexyl-{2-[3-(2-hydroxy-ethyl)-phenyl]-ethyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

2: dimethylsulfide borane complex / dichloromethane / 2 h / 20 °C / Heating / reflux

3: dichloromethane / 2 h / 20 °C

With dimethylsulfide borane complex; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;