3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid

Base Information

• Chemical Name: 3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid
• CAS No.: 1601468-79-4
• Molecular Formula: C₁₈H₁₂Cl₃N₃O₂S
• Molecular Weight: 440.737

Synonyms:3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid

Chemical Property of 3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid

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Technology Process of 3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid

There total 4 articles about 3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

4-(3,4-dichloro-phenyl)-thiazol-2-yl-hydrazine (312303-66-5) + 3-(4-chlorophenyl)-2-hydroxyacrylic acid (127273-12-5) → 3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid (1601468-79-4) + 3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid (1601468-78-3)

Guidance literature:

In ethanol; acetic acid; at 90 ℃; for 1h;

DOI:10.1016/j.ejmech.2014.03.034

Reference yield:

4-chlorobenzaldehyde (104-88-1) → 3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid (1601468-79-4) + 3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid (1601468-78-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium acetate / acetic anhydride / 4 h / Inert atmosphere; Reflux

2: hydrogenchloride / water / 2 h / Reflux; Inert atmosphere

3: acetic acid; ethanol / 1 h / 90 °C

With hydrogenchloride; sodium acetate; In ethanol; water; acetic anhydride; acetic acid;

DOI:10.1016/j.ejmech.2014.03.034

Reference yield:

2-acetamido-3-(4-chlorophenyl)acrylic acid (88681-63-4,3617-00-3) → 3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid (1601468-79-4) + 3-(4-chlorophenyl)-2-(2-(4-(3,4-dichlorophenyl)thiazol-2-yl)hydrazono)propanoic acid (1601468-78-3)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / water / 2 h / Reflux; Inert atmosphere

2: acetic acid; ethanol / 1 h / 90 °C

With hydrogenchloride; In ethanol; water; acetic acid;

DOI:10.1016/j.ejmech.2014.03.034

upstream raw materials:

4-chlorobenzaldehyde

2-acetamido-3-(4-chlorophenyl)acrylic acid

4-(3,4-dichloro-phenyl)-thiazol-2-yl-hydrazine

3-(4-chlorophenyl)-2-hydroxyacrylic acid

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