<(all-E)-2,6,10,14-Tetramethyl-16-(phenylthio)hexadeca-2,6,10,14-tetraen-1-yl>-acetat

Base Information

Chemical Name:<(all-E)-2,6,10,14-Tetramethyl-16-(phenylthio)hexadeca-2,6,10,14-tetraen-1-yl>-acetat
CAS No.:132274-01-2
Molecular Formula:C₂₈H₄₀O₂S
Molecular Weight:440.69
Hs Code.:

Synonyms:<(all-E)-2,6,10,14-Tetramethyl-16-(phenylthio)hexadeca-2,6,10,14-tetraen-1-yl>-acetat

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Chemical Property of <(all-E)-2,6,10,14-Tetramethyl-16-(phenylthio)hexadeca-2,6,10,14-tetraen-1-yl>-acetat

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Technology Process of <(all-E)-2,6,10,14-Tetramethyl-16-(phenylthio)hexadeca-2,6,10,14-tetraen-1-yl>-acetat

There total 5 articles about <(all-E)-2,6,10,14-Tetramethyl-16-(phenylthio)hexadeca-2,6,10,14-tetraen-1-yl>-acetat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 930-69-8
sodium thiophenolate

: Acetic acid (2E,6E,10E,14E)-16-bromo-2,6,10,14-tetramethyl-hexadeca-2,6,10,14-tetraenyl ester

: 132274-01-2
<(all-E)-2,6,10,14-Tetramethyl-16-(phenylthio)hexadeca-2,6,10,14-tetraen-1-yl>-acetat

Guidance literature:: In N,N-dimethyl-formamide; at 60 ℃; for 16h;
DOI:10.1002/hlca.19900730721

Reference yield:

: 1117-52-8
6,10,14-trimethyl-5,9,13-pentadecatriene-2-on

: 132274-01-2
<(all-E)-2,6,10,14-Tetramethyl-16-(phenylthio)hexadeca-2,6,10,14-tetraen-1-yl>-acetat

Guidance literature:: Multi-step reaction with 5 steps

1: 28 percent / SeO₂, tert-butyl-hydroperoxid (TBHP) / CH₂Cl₂; H₂O / 18 h / 0 °C

2: 92 percent / tetrahydrofuran / 4 h / Ambient temperature

3: 95 percent / pyridin / 2 h

4: PBr₃, pyridine / petroleum ether / 3 h / -17 °C

5: 45 percent / dimethylformamide / 16 h / 60 °C

With pyridine; tert.-butylhydroperoxide; selenium(IV) oxide; phosphorus tribromide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; Petroleum ether;
DOI:10.1002/hlca.19900730721

Reference yield:

: 132273-99-5
(all-E)-15-Hydroxy-6,10,14-trimethylpentadeca-5,9,13-trien-2-on

: 132274-01-2
<(all-E)-2,6,10,14-Tetramethyl-16-(phenylthio)hexadeca-2,6,10,14-tetraen-1-yl>-acetat

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / tetrahydrofuran / 4 h / Ambient temperature

2: 95 percent / pyridin / 2 h

3: PBr₃, pyridine / petroleum ether / 3 h / -17 °C

4: 45 percent / dimethylformamide / 16 h / 60 °C

With pyridine; phosphorus tribromide; In tetrahydrofuran; N,N-dimethyl-formamide; Petroleum ether;
DOI:10.1002/hlca.19900730721