Technology Process of C15H15F3N2O
There total 3 articles about C15H15F3N2O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
methanol;
at 40 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tert.-butyl lithium / pentane / 0 °C / Inert atmosphere
1.2: 0.5 h / -78 °C / Inert atmosphere
2.1: sodium carbonate / 1,2-dimethoxyethane; water / 0.08 h / Inert atmosphere
2.2: 16 h / 80 °C / Inert atmosphere; Sealed tube
3.1: toluene-4-sulfonic acid / methanol / 0.5 h / 40 °C
With
tert.-butyl lithium; sodium carbonate; toluene-4-sulfonic acid;
In
methanol; 1,2-dimethoxyethane; water; pentane;
2.1: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium carbonate / 1,2-dimethoxyethane; water / 0.08 h / Inert atmosphere
1.2: 16 h / 80 °C / Inert atmosphere; Sealed tube
2.1: toluene-4-sulfonic acid / methanol / 0.5 h / 40 °C
With
sodium carbonate; toluene-4-sulfonic acid;
In
methanol; 1,2-dimethoxyethane; water;
1.1: |Suzuki Coupling;