Ethanone, 1-bicyclo[2.1.0]pent-2-yl-, (1alpha,2alpha,4alpha)- (9CI)

Base Information

Chemical Name:Ethanone, 1-bicyclo[2.1.0]pent-2-yl-, (1alpha,2alpha,4alpha)- (9CI)
CAS No.:104951-19-1
Molecular Formula:C₇H₁₀O
Molecular Weight:110.156
Hs Code.:
Mol file:104951-19-1.mol

Synonyms:Ethanone,1-bicyclo[2.1.0]pent-2-yl-, (1a,2a,4a)- (9CI); Bicyclo[2.1.0]pentane, ethanone deriv.

Suppliers and Price of Ethanone, 1-bicyclo[2.1.0]pent-2-yl-, (1alpha,2alpha,4alpha)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanone, 1-bicyclo[2.1.0]pent-2-yl-, (1alpha,2alpha,4alpha)- (9CI)

Chemical Property:

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Technology Process of Ethanone, 1-bicyclo[2.1.0]pent-2-yl-, (1alpha,2alpha,4alpha)- (9CI)

There total 10 articles about Ethanone, 1-bicyclo[2.1.0]pent-2-yl-, (1alpha,2alpha,4alpha)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 917-54-4
methyllithium

: 58191-46-1,105017-01-4
exo-bicyclo<2.1.0>pentene<2.1.0>-2-carboxylic acid

: 104951-19-1,105017-00-3
endo-2-acetylbicyclo<2.1.0>pentane

Guidance literature:: In diethyl ether; at -10 ℃; for 1h;

Reference yield: 64.0%

: 917-54-4
methyllithium

: 58191-46-1,105017-01-4
endo-bicyclo<2.1.0>pentene<2.1.0>-2-carboxylic acid

: 104951-19-1,105017-00-3
exo-2-acetylbicyclo<2.1.0>pentane

Guidance literature:: In diethyl ether; at -10 ℃; for 1h;

Reference yield:

: 24810-45-5
3-diazobicyclo-[3.1.0]hexan-2-one

: 104951-19-1,105017-00-3
endo-2-acetylbicyclo<2.1.0>pentane

Guidance literature:: Multi-step reaction with 5 steps

1: 3.8 g / collidine / 180 °C

2: 64 percent / 2M NaOH / H₂O / 3 h / 55 °C

4: 0.3M NaOH / 40 h / 20 °C

5: 67 percent / diethyl ether / 1 h / -10 °C

With 2,3,5-trimethyl-pyridine; sodium hydroxide; In diethyl ether; water;