3'-Adenylicacid, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-N-benzoyl-P-(2-chlorophenyl)-2'-deoxycytidylyl-(3'®5')-N-benzoyl-2'-deoxy-,2-chlorophenyl 2-cyanoethyl ester (9CI)

Base Information

• Chemical Name: 3'-Adenylicacid, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-N-benzoyl-P-(2-chlorophenyl)-2'-deoxycytidylyl-(3'®5')-N-benzoyl-2'-deoxy-,2-chlorophenyl 2-cyanoethyl ester (9CI)
• CAS No.: 78111-50-9
• Molecular Formula: C69H61 Cl2 N9 O16 P2
• Molecular Weight: 1405.15

Synonyms:

Chemical Property of 3'-Adenylicacid, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-N-benzoyl-P-(2-chlorophenyl)-2'-deoxycytidylyl-(3'®5')-N-benzoyl-2'-deoxy-,2-chlorophenyl 2-cyanoethyl ester (9CI)

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3'-Adenylicacid, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-N-benzoyl-P-(2-chlorophenyl)-2'-deoxycytidylyl-(3'®5')-N-benzoyl-2'-deoxy-,2-chlorophenyl 2-cyanoethyl ester (9CI)

There total 7 articles about 3'-Adenylicacid, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-N-benzoyl-P-(2-chlorophenyl)-2'-deoxycytidylyl-(3'®5')-N-benzoyl-2'-deoxy-,2-chlorophenyl 2-cyanoethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide) (72351-28-1) → C69H61Cl2N9O16P2 (78111-50-9)

Guidance literature:

Multi-step reaction with 3 steps

2: H₂O / pyridine

3: mesitylenesulfonyl-3-nitrotriazolide

With mesitylenesulfonyl-3-nitrotriazolide; water; In pyridine;

DOI:10.1248/cpb.34.2202

Reference yield:

[1,2,4]Triazol-1-yl-phosphonic acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester (76964-04-0) → C69H61Cl2N9O16P2 (78111-50-9)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O / pyridine

2: mesitylenesulfonyl-3-nitrotriazolide

With mesitylenesulfonyl-3-nitrotriazolide; water; In pyridine;

DOI:10.1248/cpb.34.2202

Reference yield:

4-N-Benzoyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)cytidine (67219-55-0) → C69H61Cl2N9O16P2 (78111-50-9)

Guidance literature:

Multi-step reaction with 3 steps

2: H₂O / pyridine

3: mesitylenesulfonyl-3-nitrotriazolide

With mesitylenesulfonyl-3-nitrotriazolide; water; In pyridine;

DOI:10.1248/cpb.34.2202

upstream raw materials:

bzA_dΦ(CNEt)

N-6-benzoyl-5'-O-(dimethoxytrityl)-2'-deoxyadenosine 3'-(o-chlorophenyl β-cyanoethyl phosphate)

2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide)

[1,2,4]Triazol-1-yl-phosphonic acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester

Downstream raw materials:

C₆₆H₅₈Cl₂N₈O₁₆P₂*C₆H₁₅N

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