Bis(1H-1,2,4-triazol-1-yl)phosphinic acid 2-chlorophenyl ester

Base Information

Chemical Name:Bis(1H-1,2,4-triazol-1-yl)phosphinic acid 2-chlorophenyl ester
CAS No.:72351-28-1
Molecular Formula:C10H8ClN6O2P
Molecular Weight:310.639
Hs Code.:
DSSTox Substance ID:DTXSID60449390
Nikkaji Number:J938.232A
Wikidata:Q82268835

Synonyms:72351-28-1;AGN-PC-0NDATZ;SCHEMBL24304589;DTXSID60449390;Bis(1H-1,2,4-triazol-1-yl)phosphinic acid 2-chlorophenyl ester

Suppliers and Price of Bis(1H-1,2,4-triazol-1-yl)phosphinic acid 2-chlorophenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Bis(1H-1,2,4-triazol-1-yl)phosphinic acid 2-chlorophenyl ester

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:310.0134882
Heavy Atom Count:20
Complexity:369

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)OP(=O)(N2C=NC=N2)N3C=NC=N3)Cl

Technology Process of Bis(1H-1,2,4-triazol-1-yl)phosphinic acid 2-chlorophenyl ester

There total 1 articles about Bis(1H-1,2,4-triazol-1-yl)phosphinic acid 2-chlorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 288-88-0
1,2,4-Triazole

: 15074-54-1
2-chlorophenyl dichlorophosphate

: 72351-28-1
2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide)

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1021/jo00324a010

Reference yield:

: 72351-28-1
2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide)

: 78098-91-6
C₆₃H₅₈Cl₂N₈O₁₆P₂

Guidance literature:: Multi-step reaction with 4 steps

1: dioxane / 2 h / 20 °C

2: 1-methylimidazole / dioxane / 3 h / 20 °C

3: benzenesulfonic acid / CHCl₃; methanol / 0.25 h / 0 °C

4: 62 percent / 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole / pyridine / 3.5 h / 20 °C

With 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole; benzenesulfonic acid; 1-methyl-1H-imidazole; In 1,4-dioxane; pyridine; methanol; chloroform;
DOI:10.1002/hlca.19820650803

Reference yield:

: 72351-28-1
2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide)

: 78098-92-7
C₆₀H₆₀Cl₂N₈O₁₇P₂

Guidance literature:: Multi-step reaction with 3 steps

2: H₂O / pyridine

3: mesitylenesulfonyl-3-nitrotriazolide

With mesitylenesulfonyl-3-nitrotriazolide; water; In pyridine;
DOI:10.1248/cpb.34.2202