2-{3-[2-(3-methanesulfinyl-phenyl)-ethoxy]-4-methoxy-benzoylamino}-indane-2-carboxylic acid

Base Information

Chemical Name:2-{3-[2-(3-methanesulfinyl-phenyl)-ethoxy]-4-methoxy-benzoylamino}-indane-2-carboxylic acid
CAS No.:1195941-41-3
Molecular Formula:C₂₇H₂₇NO₆S
Molecular Weight:493.58
Hs Code.:

Synonyms:2-{3-[2-(3-methanesulfinyl-phenyl)-ethoxy]-4-methoxy-benzoylamino}-indane-2-carboxylic acid

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Chemical Property of 2-{3-[2-(3-methanesulfinyl-phenyl)-ethoxy]-4-methoxy-benzoylamino}-indane-2-carboxylic acid

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Technology Process of 2-{3-[2-(3-methanesulfinyl-phenyl)-ethoxy]-4-methoxy-benzoylamino}-indane-2-carboxylic acid

There total 6 articles about 2-{3-[2-(3-methanesulfinyl-phenyl)-ethoxy]-4-methoxy-benzoylamino}-indane-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1195941-40-2
2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid

: 1195941-41-3
2-{3-[2-(3-methanesulfinyl-phenyl)-ethoxy]-4-methoxy-benzoylamino}-indane-2-carboxylic acid

Guidance literature:: With dihydrogen peroxide; acetic acid; In water; at 20 ℃; for 2h;

Reference yield:

: 60444-56-6
3-acetoxy-4-methoxybenzoic acid

: 1195941-41-3
2-{3-[2-(3-methanesulfinyl-phenyl)-ethoxy]-4-methoxy-benzoylamino}-indane-2-carboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.33 h / 20 °C

2: sodium hydrogencarbonate / dichloromethane; water; ethyl acetate

3: methanol; potassium carbonate / 2 h / 20 °C

4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 20 °C

5: water; lithium hydroxide / 1,4-dioxane / 1 h / 60 °C

6: dihydrogen peroxide; acetic acid / water / 2 h / 20 °C

With methanol; oxalyl dichloride; di-isopropyl azodicarboxylate; water; dihydrogen peroxide; sodium hydrogencarbonate; potassium carbonate; acetic acid; triphenylphosphine; lithium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; ethyl acetate;

Reference yield:

: 90798-12-2
3-acetoxy-4-methoxy-benzoyl chloride

: 1195941-41-3
2-{3-[2-(3-methanesulfinyl-phenyl)-ethoxy]-4-methoxy-benzoylamino}-indane-2-carboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate / dichloromethane; water; ethyl acetate

2: methanol; potassium carbonate / 2 h / 20 °C

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 20 °C

4: water; lithium hydroxide / 1,4-dioxane / 1 h / 60 °C

5: dihydrogen peroxide; acetic acid / water / 2 h / 20 °C

With methanol; di-isopropyl azodicarboxylate; water; dihydrogen peroxide; sodium hydrogencarbonate; potassium carbonate; acetic acid; triphenylphosphine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; ethyl acetate;