2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid

Base Information

Chemical Name:2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid
CAS No.:1195941-40-2
Molecular Formula:C₂₇H₂₇NO₅S
Molecular Weight:477.581
Hs Code.:

Synonyms:2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid

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Chemical Property of 2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid

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Technology Process of 2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid

There total 5 articles about 2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1195941-39-9
2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid methyl ester

: 1195941-40-2
2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid

Guidance literature:: 2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid methyl ester; With water; lithium hydroxide; In 1,4-dioxane; at 60 ℃; for 1h;

With hydrogenchloride; In 1,4-dioxane; water; ethyl acetate;

Reference yield:

: 60444-56-6
3-acetoxy-4-methoxybenzoic acid

: 1195941-40-2
2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.33 h / 20 °C

2: sodium hydrogencarbonate / dichloromethane; water; ethyl acetate

3: methanol; potassium carbonate / 2 h / 20 °C

4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 20 °C

5: water; lithium hydroxide / 1,4-dioxane / 1 h / 60 °C

With methanol; oxalyl dichloride; di-isopropyl azodicarboxylate; water; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; lithium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; ethyl acetate;

Reference yield:

: 1195944-89-8
2-(3-acetoxy-4-methoxy-benzoylamino)-indane-2-carboxylic acid methyl ester

: 1195941-40-2
2-{4-methoxy-3-[2-(3-methylsulfanyl-phenyl)-ethoxy]-benzoylamino}-indane-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; potassium carbonate / 2 h / 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 20 °C

3: water; lithium hydroxide / 1,4-dioxane / 1 h / 60 °C

With methanol; di-isopropyl azodicarboxylate; water; potassium carbonate; triphenylphosphine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane;