methyl 2-carbamoyl-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propionate

Base Information

Chemical Name:methyl 2-carbamoyl-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propionate
CAS No.:199794-29-1
Molecular Formula:C₂₃H₂₄N₂O₅
Molecular Weight:408.454
Hs Code.:

Synonyms:methyl 2-carbamoyl-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propionate

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Chemical Property of methyl 2-carbamoyl-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propionate

Chemical Property:

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Technology Process of methyl 2-carbamoyl-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propionate

There total 6 articles about methyl 2-carbamoyl-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ethyl acetate n-hexane

: 199794-28-0
2-methoxycarbonyl-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propionic acid

: 199794-29-1
methyl 2-carbamoyl-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propionate

Guidance literature:: With ammonium hydroxide; thionyl chloride; In ethyl acetate; acetone; benzene;

Reference yield:

: 103788-59-6
4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]benzaldehyde

: 199794-29-1
methyl 2-carbamoyl-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propionate

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / piperidinium acetate / toluene / 4 h / Heating

2: 85 percent / H₂ / 5percent Pd/C / methanol; dioxane / Ambient temperature

3: 72 percent / 2N aq. NaOH / tetrahydrofuran; methanol / 1.5 h / Ambient temperature

4: thionyl chloride / benzene / 1.5 h / 80 °C

5: 28percent aq. NH₃ / acetone / 0.5 h / Ambient temperature

With ammonium hydroxide; sodium hydroxide; thionyl chloride; hydrogen; piperdinium acetate; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; acetone; toluene; benzene;
DOI:10.1021/jm970771m

Reference yield:

: 209530-90-5
dimethyl [4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]benzylidene]-malonate

: 199794-29-1
methyl 2-carbamoyl-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propionate

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / H₂ / 5percent Pd/C / methanol; dioxane / Ambient temperature

2: 72 percent / 2N aq. NaOH / tetrahydrofuran; methanol / 1.5 h / Ambient temperature

3: thionyl chloride / benzene / 1.5 h / 80 °C

4: 28percent aq. NH₃ / acetone / 0.5 h / Ambient temperature

With ammonium hydroxide; sodium hydroxide; thionyl chloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; acetone; benzene;
DOI:10.1021/jm970771m