1,4-bis[2,6-diisopropyl-4-(4-phenyl-1,2,3-1H-triazol-1-yl)phenyl]1,4-diazabuta-1,3-diene

Base Information

Chemical Name:1,4-bis[2,6-diisopropyl-4-(4-phenyl-1,2,3-1H-triazol-1-yl)phenyl]1,4-diazabuta-1,3-diene
CAS No.:1379662-54-0
Molecular Formula:C₄₂H₄₆N₈
Molecular Weight:662.881
Hs Code.:

Synonyms:1,4-bis[2,6-diisopropyl-4-(4-phenyl-1,2,3-1H-triazol-1-yl)phenyl]1,4-diazabuta-1,3-diene

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Chemical Property of 1,4-bis[2,6-diisopropyl-4-(4-phenyl-1,2,3-1H-triazol-1-yl)phenyl]1,4-diazabuta-1,3-diene

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Technology Process of 1,4-bis[2,6-diisopropyl-4-(4-phenyl-1,2,3-1H-triazol-1-yl)phenyl]1,4-diazabuta-1,3-diene

There total 4 articles about 1,4-bis[2,6-diisopropyl-4-(4-phenyl-1,2,3-1H-triazol-1-yl)phenyl]1,4-diazabuta-1,3-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1379662-50-6
1,4-bis(4-azido-2,6-diisopropylphenyl)-1,4-diazabuta-1,3-diene

: 536-74-3
phenylacetylene

: 1379662-54-0
1,4-bis[2,6-diisopropyl-4-(4-phenyl-1,2,3-1H-triazol-1-yl)phenyl]1,4-diazabuta-1,3-diene

Guidance literature:: With [Cu(4,7-dichloro-1,10-phenanthroline)(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)]; In methanol; at 60 ℃;
DOI:10.1039/c2dt30249g

Reference yield:

: 1379662-49-3
4-azido-2,6-diisopropylaniline

: 1379662-54-0
1,4-bis[2,6-diisopropyl-4-(4-phenyl-1,2,3-1H-triazol-1-yl)phenyl]1,4-diazabuta-1,3-diene

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / methanol; water / 4 h / 20 °C

2: [Cu(4,7-dichloro-1,10-phenanthroline)(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)] / methanol / 60 °C

With [Cu(4,7-dichloro-1,10-phenanthroline)(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)]; acetic acid; In methanol; water;
DOI:10.1039/c2dt30249g

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1379662-54-0
1,4-bis[2,6-diisopropyl-4-(4-phenyl-1,2,3-1H-triazol-1-yl)phenyl]1,4-diazabuta-1,3-diene

Guidance literature:: Multi-step reaction with 4 steps

1: iodine; sodium hydrogencarbonate / diethyl ether; water / 2 h

2: copper(l) iodide; sodium azide; Vitamin C; sodium hydroxide; N,N`-dimethylethylenediamine / water; dimethyl sulfoxide / 50 °C / Inert atmosphere

3: acetic acid / methanol; water / 4 h / 20 °C

4: [Cu(4,7-dichloro-1,10-phenanthroline)(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)] / methanol / 60 °C

With copper(l) iodide; sodium azide; [Cu(4,7-dichloro-1,10-phenanthroline)(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)]; Vitamin C; iodine; sodium hydrogencarbonate; acetic acid; sodium hydroxide; N,N`-dimethylethylenediamine; In methanol; diethyl ether; water; dimethyl sulfoxide;
DOI:10.1039/c2dt30249g