(R)-2-[4-(4-chloro-phenyl)-thiazol-2-yl]-piperidinium trifluoroacetate

Base Information

Chemical Name:(R)-2-[4-(4-chloro-phenyl)-thiazol-2-yl]-piperidinium trifluoroacetate
CAS No.:1089729-80-5
Molecular Formula:C₂HF₃O₂*C₁₄H₁₅ClN₂S
Molecular Weight:392.829
Hs Code.:

Synonyms:(R)-2-[4-(4-chloro-phenyl)-thiazol-2-yl]-piperidinium trifluoroacetate

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Chemical Property of (R)-2-[4-(4-chloro-phenyl)-thiazol-2-yl]-piperidinium trifluoroacetate

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Technology Process of (R)-2-[4-(4-chloro-phenyl)-thiazol-2-yl]-piperidinium trifluoroacetate

There total 3 articles about (R)-2-[4-(4-chloro-phenyl)-thiazol-2-yl]-piperidinium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1089729-73-6
(R)-2-[4-(4-chloro-phenyl)-thiazol-2-yl]-piperidine-1-carboxylic acid tert-butyl ester

: 76-05-1
trifluoroacetic acid

: 1089729-80-5
(R)-2-[4-(4-chloro-phenyl)-thiazol-2-yl]-piperidinium trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 848488-91-5
tert-butyl (R)-2-carbamoylpiperidine-1-carboxyl-ate

: 1089729-80-5
(R)-2-[4-(4-chloro-phenyl)-thiazol-2-yl]-piperidinium trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: Lawessons reagent / 1,4-dioxane / 20 °C

2.1: sodium hydrogencarbonate / 1,2-dimethoxyethane / 24 h / 20 °C

2.2: 0.5 h / 0 - 20 °C

3.1: dichloromethane / 0.5 h / 20 °C

With Lawessons reagent; sodium hydrogencarbonate; In 1,4-dioxane; 1,2-dimethoxyethane; dichloromethane;

Reference yield:

: 28697-17-8
N-BOC-D-pipecolic acid

: 1089729-80-5
(R)-2-[4-(4-chloro-phenyl)-thiazol-2-yl]-piperidinium trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium chloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 1.5 h / 20 °C

2.1: Lawessons reagent / 1,4-dioxane / 20 °C

3.1: sodium hydrogencarbonate / 1,2-dimethoxyethane / 24 h / 20 °C

3.2: 0.5 h / 0 - 20 °C

4.1: dichloromethane / 0.5 h / 20 °C

With Lawessons reagent; sodium hydrogencarbonate; ammonium chloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl acetamide;