4-Methoxy-5-methyl-2-methylthio-7-(2',3',5'-tri-O-benzyl-β-D-ribofuranosyl)pyrrolo<2,3-d>pyrimidin

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Chemical Name:4-Methoxy-5-methyl-2-methylthio-7-(2',3',5'-tri-O-benzyl-β-D-ribofuranosyl)pyrrolo<2,3-d>pyrimidin
CAS No.:64609-34-3
Molecular Formula:C₃₅H₃₇N₃O₅S
Molecular Weight:611.762
Hs Code.:

Synonyms:4-Methoxy-5-methyl-2-methylthio-7-(2',3',5'-tri-O-benzyl-β-D-ribofuranosyl)pyrrolo<2,3-d>pyrimidin

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Chemical Property of 4-Methoxy-5-methyl-2-methylthio-7-(2',3',5'-tri-O-benzyl-β-D-ribofuranosyl)pyrrolo<2,3-d>pyrimidin

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Technology Process of 4-Methoxy-5-methyl-2-methylthio-7-(2',3',5'-tri-O-benzyl-β-D-ribofuranosyl)pyrrolo<2,3-d>pyrimidin

There total 3 articles about 4-Methoxy-5-methyl-2-methylthio-7-(2',3',5'-tri-O-benzyl-β-D-ribofuranosyl)pyrrolo<2,3-d>pyrimidin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75172-84-8
2,3,5-tri-O-benzyl-1-O-(p-nitrobenzoyl)-α,β-D-ribofuranose

: 64609-34-3
4-Methoxy-5-methyl-2-methylthio-7-(2',3',5'-tri-O-benzyl-β-D-ribofuranosyl)pyrrolo<2,3-d>pyrimidin

Guidance literature:: Multi-step reaction with 2 steps

1: HBr(gas.) / CH₂Cl₂

2: 1) benzyltriethylammonium chloride, aq. NaOH (50percent) / 1) 1,2-dimethoxyethane, room temp., 10 min, 2) benzene, room temp., 3 h

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; hydrogen bromide; In dichloromethane;

Reference yield:

: 57378-89-9
2,3,5-tri-O-benzyl-D-ribofuranosyl bromide

: 64609-33-2
4-methoxy-5-methyl-2-methylsulfanyl-7H-pyrrolo[2,3-d]pyrimidine

: 64609-35-4
4-Methoxy-5-methyl-2-methylthio-7-(2',3',5'-tri-O-benzyl-α-D-ribofuranosyl)pyrrolo<2,3-d>pyrimidin

: 64609-34-3
4-Methoxy-5-methyl-2-methylthio-7-(2',3',5'-tri-O-benzyl-β-D-ribofuranosyl)pyrrolo<2,3-d>pyrimidin

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; Yield given. Multistep reaction. Yields of byproduct given; 1) 1,2-dimethoxyethane, room temp., 10 min, 2) benzene, room temp., 3 h;

Reference yield:

: 64609-34-3
4-Methoxy-5-methyl-2-methylthio-7-(2',3',5'-tri-O-benzyl-β-D-ribofuranosyl)pyrrolo<2,3-d>pyrimidin

Guidance literature:: aus dem Anion von 4-Methoxy-5-methyl-2-methylthiopyrrolo<2,3-d>pyrimidin mit 2,3,5-Tri-O-benzyl-D-ribofuranosyl-bromid;
DOI:10.1016/S0040-4039(01)83424-9